1,1'-bis(pentafluorophenyl)cobaltocene

Base Information

Chemical Name:1,1'-bis(pentafluorophenyl)cobaltocene
CAS No.:320425-43-2
Molecular Formula:C₂₂H₈CoF₁₀
Molecular Weight:521.283
Hs Code.:

Synonyms:1,1'-bis(pentafluorophenyl)cobaltocene

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Chemical Property of 1,1'-bis(pentafluorophenyl)cobaltocene

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Technology Process of 1,1'-bis(pentafluorophenyl)cobaltocene

There total 1 articles about 1,1'-bis(pentafluorophenyl)cobaltocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: cobalt(II) bromide

: sodium (pentafluorophenyl)cyclopentadienide

: 320425-43-2
1,1'-bis(pentafluorophenyl)cobaltocene

Guidance literature:: In tetrahydrofuran; under inert atm., CoBr2 and Na-compd. (1:2 molar ratio) were refluxed for 2 h in thf; solvent was evapd., residue was extd. with toluene, mixt. was filtered, filtrate was evapd., solid was subsequently crystd. from pentane at -20 °C; subl. at 100-120 °C/0.050 Torr, elem. anal.;
DOI:10.1021/om000798v

Reference yield: 86.0%

: 17084-13-8
potassium hexafluorophosphate

: 320425-43-2
1,1'-bis(pentafluorophenyl)cobaltocene

: 320425-50-1
bis[η(5)-pentafluorophenylcyclopentadienyl]cobalt(III) hexafluorophosphate

Guidance literature:: With O₂; In hydrogenchloride; water; toluene; air was bubbled into a 12 M aq. HCl-toluene biphasic soln.. until color of org. phase disappeared, layers were sepd., aq. KPF6 was added; ppt. was filtered, dried in vac. desiccator over anhyd. CaSO4, elem. anal.;
DOI:10.1021/om000798v