Cyclohexanesulfinic acid (1S,2R)-1-phenyl-2-(toluene-4-sulfonylamino)-propyl ester

Base Information

Chemical Name:Cyclohexanesulfinic acid (1S,2R)-1-phenyl-2-(toluene-4-sulfonylamino)-propyl ester
CAS No.:861821-87-6
Molecular Formula:C₂₂H₂₉NO₄S₂
Molecular Weight:435.609
Hs Code.:

Synonyms:Cyclohexanesulfinic acid (1S,2R)-1-phenyl-2-(toluene-4-sulfonylamino)-propyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclohexanesulfinic acid (1S,2R)-1-phenyl-2-(toluene-4-sulfonylamino)-propyl ester

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Technology Process of Cyclohexanesulfinic acid (1S,2R)-1-phenyl-2-(toluene-4-sulfonylamino)-propyl ester

There total 1 articles about Cyclohexanesulfinic acid (1S,2R)-1-phenyl-2-(toluene-4-sulfonylamino)-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 473554-13-1
(2S,4R,5S)-N-tosyl-4-methyl-5-phenyl-1,2,3-oxathiazolidine-2-oxide

: 931-51-1
cyclohexylmagnesiumchloride

: 861821-87-6
Cyclohexanesulfinic acid (1S,2R)-1-phenyl-2-(toluene-4-sulfonylamino)-propyl ester

Guidance literature:: In tetrahydrofuran; at -78 ℃;
DOI:10.1016/j.tet.2005.03.122

Reference yield: 90.0%

: 861821-87-6
Cyclohexanesulfinic acid (1S,2R)-1-phenyl-2-(toluene-4-sulfonylamino)-propyl ester

: 16750-63-3
2-methoxyphenylmagnesium bromide

: (R)-cyclohexyl-2-methoxyphenyl-sulfoxide

: 58107-41-8,58107-43-0,108591-33-9,131142-88-6,143957-01-1,136173-99-4
N-[(1R,2S)-2-hydroxy-1-methyl-2-phenylethyl]-4-methylbenzenesulfonamide

Guidance literature:: In tetrahydrofuran; at -78 - -15 ℃;
DOI:10.1016/j.tet.2005.03.122

Reference yield:

: 861821-87-6
Cyclohexanesulfinic acid (1S,2R)-1-phenyl-2-(toluene-4-sulfonylamino)-propyl ester

: 473554-13-1
(2S,4R,5S)-N-tosyl-4-methyl-5-phenyl-1,2,3-oxathiazolidine-2-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / -78 - -15 °C

2: 95 percent / thionyl chloride; pyridine / tetrahydrofuran / -78 - -45 °C

With pyridine; thionyl chloride; In tetrahydrofuran;
DOI:10.1016/j.tet.2005.03.122