[4-(3-{4'-[3-(4-Carboxymethoxy-3-methoxy-phenylsulfanyl)-propyl]-biphenyl-4-yl}-propyl-sulfanyl)-2-methoxy-phenoxy]-acetic acid

Base Information

Chemical Name:[4-(3-{4'-[3-(4-Carboxymethoxy-3-methoxy-phenylsulfanyl)-propyl]-biphenyl-4-yl}-propyl-sulfanyl)-2-methoxy-phenoxy]-acetic acid
CAS No.:719293-63-7
Molecular Formula:C₃₆H₃₈O₈S₂
Molecular Weight:662.825
Hs Code.:

Synonyms:[4-(3-{4'-[3-(4-Carboxymethoxy-3-methoxy-phenylsulfanyl)-propyl]-biphenyl-4-yl}-propyl-sulfanyl)-2-methoxy-phenoxy]-acetic acid

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Chemical Property of [4-(3-{4'-[3-(4-Carboxymethoxy-3-methoxy-phenylsulfanyl)-propyl]-biphenyl-4-yl}-propyl-sulfanyl)-2-methoxy-phenoxy]-acetic acid

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Technology Process of [4-(3-{4'-[3-(4-Carboxymethoxy-3-methoxy-phenylsulfanyl)-propyl]-biphenyl-4-yl}-propyl-sulfanyl)-2-methoxy-phenoxy]-acetic acid

There total 10 articles about [4-(3-{4'-[3-(4-Carboxymethoxy-3-methoxy-phenylsulfanyl)-propyl]-biphenyl-4-yl}-propyl-sulfanyl)-2-methoxy-phenoxy]-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: [4-(3-{4'-[3-(4-carboxymethoxy-3-methoxy-phenylsulfanyl)-propyl]-biphenyl-4-yl}-propylsulfanyl)-2-methoxy-phenoxy]-acetic acid diethyl ester

: 719293-63-7
[4-(3-{4'-[3-(4-Carboxymethoxy-3-methoxy-phenylsulfanyl)-propyl]-biphenyl-4-yl}-propyl-sulfanyl)-2-methoxy-phenoxy]-acetic acid

Guidance literature:: With sodium hydroxide; water; In tetrahydrofuran; ethanol; at 20 ℃; for 48h;

Reference yield:

: 685139-54-2
(4-Mercapto-2-methoxy-phenoxy)-acetic acid methyl ester

: 4,4'-biphenyidipropanol bismethanesulfonate

: 78-93-3
butanone

: 719293-63-7
[4-(3-{4'-[3-(4-Carboxymethoxy-3-methoxy-phenylsulfanyl)-propyl]-biphenyl-4-yl}-propyl-sulfanyl)-2-methoxy-phenoxy]-acetic acid

Guidance literature:: With potassium carbonate; In water; ethyl acetate;

Reference yield:

: 36649-80-6
4,4'-diiodo-3,3'-dichloro-1,1'-biphenyl

: 719293-63-7
[4-(3-{4'-[3-(4-Carboxymethoxy-3-methoxy-phenylsulfanyl)-propyl]-biphenyl-4-yl}-propyl-sulfanyl)-2-methoxy-phenoxy]-acetic acid

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / palladium diacetate; triphenylphosphine / DMF (N,N-dimethyl-formamide) / 110 °C / Heating / reflux

2.1: sodium hydroxide / 1,4-dioxane; water / 4 h / Heating / reflux

2.2: 6 h

3.1: sodium tetrahydroborate / tetrahydrofuran / 0.5 h

3.2: 8 h / Heating / reflux

4.1: triethylamine / dichloromethane

5.1: potassium carbonate / butanone / 8 h / Heating / reflux

6.1: sodium hydroxide; water / tetrahydrofuran; ethanol / 48 h / 20 °C

With sodium hydroxide; sodium tetrahydroborate; water; potassium carbonate; triethylamine; palladium diacetate; triphenylphosphine; In tetrahydrofuran; 1,4-dioxane; DMF (N,N-dimethyl-formamide); ethanol; dichloromethane; water; butanone;