Benzyl (1S,2S,3S,6R)-6-(phenoxyacetylamino)<2-β-(2)H3>penicillanate 1-oxide

Base Information

Chemical Name:Benzyl (1S,2S,3S,6R)-6-(phenoxyacetylamino)<2-β-(2)H3>penicillanate 1-oxide
CAS No.:124176-53-0
Molecular Formula:C₂₃H₂₄N₂O₆S
Molecular Weight:459.496
Hs Code.:

Synonyms:Benzyl (1S,2S,3S,6R)-6-(phenoxyacetylamino)<2-β-(2)H3>penicillanate 1-oxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzyl (1S,2S,3S,6R)-6-(phenoxyacetylamino)<2-β-(2)H3>penicillanate 1-oxide

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Technology Process of Benzyl (1S,2S,3S,6R)-6-(phenoxyacetylamino)<2-β-(2)H3>penicillanate 1-oxide

There total 1 articles about Benzyl (1S,2S,3S,6R)-6-(phenoxyacetylamino)<2-β-(2)H3>penicillanate 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 42879-04-9
Benzyl (1S,3S,6R)-6-(phenoxyacetylamino)penicillanate 1-oxide

: 124176-53-0
Benzyl (1S,2S,3S,6R)-6-(phenoxyacetylamino)<2-β-(2)H3>penicillanate 1-oxide

Guidance literature:: With water-d2; In toluene; at 80 ℃; for 48h;
DOI:10.1055/s-1993-25875

Reference yield: 94.0%

: 124176-53-0
Benzyl (1S,2S,3S,6R)-6-(phenoxyacetylamino)<2-β-(2)H3>penicillanate 1-oxide

: 148680-07-3
(1S,2S,3S,6R)-6-(Phenoxyacetylamino)<2-β-(2)H3>penicillanic acid 1-oxide

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 24h; under 2585.7 Torr; Ambient temperature;
DOI:10.1055/s-1993-25875

Reference yield:

: 124176-53-0
Benzyl (1S,2S,3S,6R)-6-(phenoxyacetylamino)<2-β-(2)H3>penicillanate 1-oxide

: 124176-55-2
(2S,3S,6R)-6-(Phenoxyacetylamino)<2-β-(2)H3>penicillanic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / H₂ / 10percent Pd/C / ethyl acetate / 24 h / 2585.7 Torr / Ambient temperature

2: 88 percent / PBr₃ / dimethylformamide / 0.67 h / T < 5 deg C

With hydrogen; phosphorus tribromide; palladium on activated charcoal; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1055/s-1993-25875