5-(2-(6-(O-benzyl-L-serinamido)hexylamino)-2-oxoethyl)-2'-deoxyuridine 5'-triphosphate

Base Information

Chemical Name:5-(2-(6-(O-benzyl-L-serinamido)hexylamino)-2-oxoethyl)-2'-deoxyuridine 5'-triphosphate
CAS No.:503129-98-4
Molecular Formula:C₂₇H₄₂N₅O₁₇P₃
Molecular Weight:801.575
Hs Code.:

Synonyms:5-(2-(6-(O-benzyl-L-serinamido)hexylamino)-2-oxoethyl)-2'-deoxyuridine 5'-triphosphate

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Chemical Property of 5-(2-(6-(O-benzyl-L-serinamido)hexylamino)-2-oxoethyl)-2'-deoxyuridine 5'-triphosphate

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Technology Process of 5-(2-(6-(O-benzyl-L-serinamido)hexylamino)-2-oxoethyl)-2'-deoxyuridine 5'-triphosphate

There total 3 articles about 5-(2-(6-(O-benzyl-L-serinamido)hexylamino)-2-oxoethyl)-2'-deoxyuridine 5'-triphosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 885109-37-5
5-(2-(6-(N^α-carbobenzoxy-O-benzyl-L-serinamido)hexylamino)-2-oxoethyl)-2'-dUTP

: 503129-98-4
5-(2-(6-(O-benzyl-L-serinamido)hexylamino)-2-oxoethyl)-2'-deoxyuridine 5'-triphosphate

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; water; at 20 ℃; for 3h;
DOI:10.1016/j.bmc.2005.11.030

Reference yield:

: 20806-43-3
Z-Ser(Bzl)-OH

: 503129-98-4
5-(2-(6-(O-benzyl-L-serinamido)hexylamino)-2-oxoethyl)-2'-deoxyuridine 5'-triphosphate

Guidance literature:: Multi-step reaction with 3 steps

1: N,N'-dicyclohexylcarbodiimide / dimethylformamide / 0 - 20 °C

2: 54 percent / NaHCO₃ / dimethylformamide; H₂O / 20 °C

3: 22 percent / H₂ / Pd/C / methanol; H₂O / 3 h / 20 °C

With hydrogen; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2005.11.030

Reference yield:

: 98647-23-5
O-benzyl-N^α-benzyloxycarbonylserine succinimidyl ester

: 503129-98-4
5-(2-(6-(O-benzyl-L-serinamido)hexylamino)-2-oxoethyl)-2'-deoxyuridine 5'-triphosphate

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / NaHCO₃ / dimethylformamide; H₂O / 20 °C

2: 22 percent / H₂ / Pd/C / methanol; H₂O / 3 h / 20 °C

With hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2005.11.030