tetrabutylammonium (E)-1-(2-trimethylsilylethylseleno)-2-phenyl-1-propenethiolate

Base Information

Chemical Name:tetrabutylammonium (E)-1-(2-trimethylsilylethylseleno)-2-phenyl-1-propenethiolate
CAS No.:1415241-14-3
Molecular Formula:C₁₄H₂₁SSeSi*C₁₆H₃₆N
Molecular Weight:570.901
Hs Code.:

Synonyms:tetrabutylammonium (E)-1-(2-trimethylsilylethylseleno)-2-phenyl-1-propenethiolate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tetrabutylammonium (E)-1-(2-trimethylsilylethylseleno)-2-phenyl-1-propenethiolate

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Technology Process of tetrabutylammonium (E)-1-(2-trimethylsilylethylseleno)-2-phenyl-1-propenethiolate

There total 4 articles about tetrabutylammonium (E)-1-(2-trimethylsilylethylseleno)-2-phenyl-1-propenethiolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1415241-06-3
DL-2-phenylpropaneselenothioic acid Se-2-(trimethylsilyl)ethyl ester

: 429-41-4
tetrabutyl ammonium fluoride

: 1415241-14-3
tetrabutylammonium (E)-1-(2-trimethylsilylethylseleno)-2-phenyl-1-propenethiolate

: 1415241-17-6
tetrabutylammonium (Z)-1-(2-trimethylsilylethylseleno)-2-phenyl-1-propenethioalte

Guidance literature:: In tetrahydrofuran; at 0 ℃; for 0.5h;
DOI:10.1016/j.tet.2012.06.076 DOI:10.1016/j.tet.2012.06.076

Reference yield:

: 1415241-04-1
C₁₀H₁₂OS

: 1415241-14-3
tetrabutylammonium (E)-1-(2-trimethylsilylethylseleno)-2-phenyl-1-propenethiolate

: 1415241-17-6
tetrabutylammonium (Z)-1-(2-trimethylsilylethylseleno)-2-phenyl-1-propenethioalte

Guidance literature:: Multi-step reaction with 2 steps

1: 5,5-dimethyl-1,3-cyclohexadiene; hexane / 0 - 180 °C

2: tetrahydrofuran / 0.5 h / 0 °C

In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; hexane;
DOI:10.1016/j.tet.2012.06.076 DOI:10.1016/j.tet.2012.06.076

Reference yield:

: 439675-12-4
bis[2-(trimethylsilyl)ethyl]-diselenide

: 1415241-14-3
tetrabutylammonium (E)-1-(2-trimethylsilylethylseleno)-2-phenyl-1-propenethiolate

: 1415241-17-6
tetrabutylammonium (Z)-1-(2-trimethylsilylethylseleno)-2-phenyl-1-propenethioalte

Guidance literature:: Multi-step reaction with 3 steps

1: 5,5-dimethyl-1,3-cyclohexadiene / 0.25 h / 0 - 25 °C

2: 5,5-dimethyl-1,3-cyclohexadiene; hexane / 0 - 180 °C

3: tetrahydrofuran / 0.5 h / 0 °C

In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; hexane;
DOI:10.1016/j.tet.2012.06.076 DOI:10.1016/j.tet.2012.06.076