2-ethanol

Base Information

Chemical Name:2-ethanol
CAS No.:118261-61-3
Molecular Formula:C₁₆H₁₇Cl₂NO
Molecular Weight:310.223
Hs Code.:

2-<N-benzyl-N-(3,4-dichlorobenzyl)amino>ethanol

Synonyms:2-ethanol

Suppliers and Price of 2-ethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-ethanol

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Technology Process of 2-ethanol

There total 1 articles about 2-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 102-47-6
3,4-Dichlorophenylmethyl chloride

: 104-63-2
N-Benzylethanolamine

: 118261-61-3
2-ethanol

Guidance literature:: With hydrogenchloride; potassium carbonate; In N-methyl-acetamide;

Reference yield:

: 118261-61-3
2-ethanol

: 4-{2-[Benzyl-(3,4-dichloro-benzyl)-amino]-ethoxy}-2-[1-(2-nitro-phenyl)-meth-(Z)-ylidene]-3-oxo-butyric acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) THF, 40 deg C, 30 min, 2.) THF, room temperature, 15 h

2: 1.50 g / piperidine / benzene / 14 h / Heating

With piperidine; sodium hydride; In benzene;
DOI:10.1021/jm00130a029

Reference yield:

: 118261-61-3
2-ethanol

: 122567-92-4
4-{2-[Benzyl-(3,4-dichloro-benzyl)-amino]-ethoxymethyl}-2-methyl-6-(2-nitro-phenyl)-1,6-dihydro-pyrimidine-5-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaH / 1.) THF, 40 deg C, 30 min, 2.) THF, room temperature, 15 h

2: 1.50 g / piperidine / benzene / 14 h / Heating

3: 1.) t-BuOK, 2.) p-toluenesulfonic acid monohydrate / 1.) DMF, a) 0 deg C, 1 h, b) room temperature, 3 h, 2.) DMF, 110 deg C, 3 h

With piperidine; potassium tert-butylate; sodium hydride; toluene-4-sulfonic acid; In benzene;
DOI:10.1021/jm00130a029