C₃₂H₃₉NO₅Si

Base Information

Chemical Name:C₃₂H₃₉NO₅Si
CAS No.:1267651-86-4
Molecular Formula:C₃₂H₃₉NO₅Si
Molecular Weight:545.751
Hs Code.:

C<sub>32</sub>H<sub>39</sub>NO<sub>5</sub>Si

Synonyms:C₃₂H₃₉NO₅Si

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Chemical Property of C₃₂H₃₉NO₅Si

Chemical Property:

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Technology Process of C₃₂H₃₉NO₅Si

There total 10 articles about C₃₂H₃₉NO₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 870137-18-1
(R)-4-((R)-1-hydroxy-1-methylprop-2-ynyl)-2,2-dimethyl-oxazolidine-3-carboxylic acid tert-butyl ester

: 1267651-86-4
C₃₂H₃₉NO₅Si

Guidance literature:: Multi-step reaction with 8 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

2: 1,4-bis-(9-O-dihydroquinidinyl)phthalazine; methanesulfonamide / water; tert-butyl alcohol / 24 h / 20 °C

3: dmap; triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere

4: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 12 h / 50 °C / Inert atmosphere

5: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

6: toluene-4-sulfonic acid / methanol / 2 h / 20 °C

7: Dess-Martin periodane / dichloromethane / 1 h / 20 °C

8: tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With dmap; 1,4-bis-(9-O-dihydroquinidinyl)phthalazine; lithium aluminium tetrahydride; methanesulfonamide; sodium hexamethyldisilazane; tetra-(n-butyl)ammonium iodide; Dess-Martin periodane; toluene-4-sulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; water; 1,2-dichloro-ethane; tert-butyl alcohol;
DOI:10.1021/ol103094j

Reference yield:

: 1267651-79-5
C₃₀H₄₅NO₆Si

: 1267651-86-4
C₃₂H₃₉NO₅Si

Guidance literature:: Multi-step reaction with 5 steps

1: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 12 h / 50 °C / Inert atmosphere

2: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

3: toluene-4-sulfonic acid / methanol / 2 h / 20 °C

4: Dess-Martin periodane / dichloromethane / 1 h / 20 °C

5: tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With sodium hexamethyldisilazane; tetra-(n-butyl)ammonium iodide; Dess-Martin periodane; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1021/ol103094j

Reference yield:

: 1267651-84-2
C₃₄H₄₃NO₆Si

: 1267651-86-4
C₃₂H₃₉NO₅Si

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / methanol / 2 h / 20 °C

2: Dess-Martin periodane / dichloromethane / 1 h / 20 °C

3: tetrahydrofuran / 0 - 20 °C / Inert atmosphere

With Dess-Martin periodane; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/ol103094j