(Pd(1,4-dichloro-2,3-benzenedithiolate))2(μ-1,2-bis(diphenylphosphino)acetylene)2

Base Information

Chemical Name:(Pd(1,4-dichloro-2,3-benzenedithiolate))2(μ-1,2-bis(diphenylphosphino)acetylene)2
CAS No.:1146360-15-7
Molecular Formula:C₆₄H₄₄Cl₄P₄Pd₂S₄
Molecular Weight:1419.86
Hs Code.:

Synonyms:(Pd(1,4-dichloro-2,3-benzenedithiolate))2(μ-1,2-bis(diphenylphosphino)acetylene)2

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Chemical Property of (Pd(1,4-dichloro-2,3-benzenedithiolate))2(μ-1,2-bis(diphenylphosphino)acetylene)2

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Technology Process of (Pd(1,4-dichloro-2,3-benzenedithiolate))2(μ-1,2-bis(diphenylphosphino)acetylene)2

There total 3 articles about (Pd(1,4-dichloro-2,3-benzenedithiolate))2(μ-1,2-bis(diphenylphosphino)acetylene)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87314-49-6
3,6-dichlorobenzene-1,2-dithiol

: [Pd₂Cl₄(1,2-bis(diphenylphosphino)acetylene)2] * 2 CHCl₃

: 1146360-15-7
(Pd(1,4-dichloro-2,3-benzenedithiolate))2(μ-1,2-bis(diphenylphosphino)acetylene)2

Guidance literature:: In chloroform; (protected from light and air, under Ar); ligand dissolved in CHCl3 added to CHCl3 soln. of Pd-complex, stirred for 2 h; dried under reduced pressure, recrystd. from CHCl3, MeOH or CH2Cl2-MeOH;elem. anal.;
DOI:10.1039/b815013c

Reference yield:

: 87314-49-6
3,6-dichlorobenzene-1,2-dithiol

: (Pd(OTf)2)2(μ-1,2-bis(diphenylphosphino)acetylene)2

: 1146360-15-7
(Pd(1,4-dichloro-2,3-benzenedithiolate))2(μ-1,2-bis(diphenylphosphino)acetylene)2

Guidance literature:: In nitromethane; chloroform; (protected from light and air, under Ar); ligand dissolved in CHCl3 added to nitromethane soln. of Pd-complex, stirred for 2 h; dried under reduced pressure, recrystd. from CHCl3, MeOH or CH2Cl2-MeOH;
DOI:10.1039/b815013c