N,N'-Diphenyl-S-(1,4-diphenyl-6-thioxo-1,6-dihydro-1,3,5-triazinyl)isothiouronium dihydrochloride

Base Information

Chemical Name:N,N'-Diphenyl-S-(1,4-diphenyl-6-thioxo-1,6-dihydro-1,3,5-triazinyl)isothiouronium dihydrochloride
CAS No.:85442-60-0
Molecular Formula:C₂₈H₂₁N₅S₂*2ClH
Molecular Weight:564.562
Hs Code.:

Synonyms:N,N'-Diphenyl-S-(1,4-diphenyl-6-thioxo-1,6-dihydro-1,3,5-triazinyl)isothiouronium dihydrochloride

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Chemical Property of N,N'-Diphenyl-S-(1,4-diphenyl-6-thioxo-1,6-dihydro-1,3,5-triazinyl)isothiouronium dihydrochloride

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Technology Process of N,N'-Diphenyl-S-(1,4-diphenyl-6-thioxo-1,6-dihydro-1,3,5-triazinyl)isothiouronium dihydrochloride

There total 2 articles about N,N'-Diphenyl-S-(1,4-diphenyl-6-thioxo-1,6-dihydro-1,3,5-triazinyl)isothiouronium dihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 85442-34-8
1,4-Diphenyl-2-mercapto-1,6-dihydro-1,3,5-triazine-6-thione

: 622-16-2
1,3-Diphenylcarbodiimide

: 85442-60-0
N,N'-Diphenyl-S-(1,4-diphenyl-6-thioxo-1,6-dihydro-1,3,5-triazinyl)isothiouronium dihydrochloride

Guidance literature:: With hydrogenchloride; In acetone; for 0.5h;
DOI:10.1021/je00034a021

Reference yield:

: 39543-11-8
2-(Benzylmercapto)-1,4-diphenyl-1,6-dihydro-1,3,5-triazine-6-thione

: 85442-60-0
N,N'-Diphenyl-S-(1,4-diphenyl-6-thioxo-1,6-dihydro-1,3,5-triazinyl)isothiouronium dihydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / thiourea, conc. hydrochloric acid / ethanol / 2.5 h / Heating

2: 65 percent / HCl / acetone / 0.5 h

With hydrogenchloride; thiourea; In ethanol; acetone;
DOI:10.1021/je00034a021