1-<5-<3-(N-cyclohexyl-N-methylcarbamoyl)propoxy>-2-nitrobenzyl>hydantoin

Base Information

Chemical Name:1-<5-<3-(N-cyclohexyl-N-methylcarbamoyl)propoxy>-2-nitrobenzyl>hydantoin
CAS No.:116005-72-2
Molecular Formula:C₂₁H₂₈N₄O₆
Molecular Weight:432.477
Hs Code.:

Synonyms:1-<5-<3-(N-cyclohexyl-N-methylcarbamoyl)propoxy>-2-nitrobenzyl>hydantoin

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Chemical Property of 1-<5-<3-(N-cyclohexyl-N-methylcarbamoyl)propoxy>-2-nitrobenzyl>hydantoin

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Technology Process of 1-<5-<3-(N-cyclohexyl-N-methylcarbamoyl)propoxy>-2-nitrobenzyl>hydantoin

There total 3 articles about 1-<5-<3-(N-cyclohexyl-N-methylcarbamoyl)propoxy>-2-nitrobenzyl>hydantoin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 116005-71-1
(2-{5-[3-(Cyclohexyl-methyl-carbamoyl)-propoxy]-2-nitro-benzylamino}-acetyl)-carbamic acid methyl ester

: 116005-72-2
1-<5-<3-(N-cyclohexyl-N-methylcarbamoyl)propoxy>-2-nitrobenzyl>hydantoin

Guidance literature:: With sodium methylate; In methanol; for 18h; Heating;
DOI:10.1021/jm00119a015

Reference yield:

: 94193-38-1
N-Cyclohexyl-N-methyl-4-(3-formyl-4-nitrophenyl)-oxybutyramide

: 116005-72-2
1-<5-<3-(N-cyclohexyl-N-methylcarbamoyl)propoxy>-2-nitrobenzyl>hydantoin

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / 1.) sodium acetate, 2.) sodium cyanoborohydride / 1.) methanol, reflux, 2.) room temperature, 3 h

2: triethylamine / tetrahydrofuran / Ambient temperature

3: 60 percent / sodium methoxide / methanol / 18 h / Heating

With sodium methylate; sodium acetate; sodium cyanoborohydride; triethylamine; In tetrahydrofuran; methanol;
DOI:10.1021/jm00119a015

Reference yield:

: 116005-70-0
N-cyclohexyl-N-methyl-4-<3-<<(carbamoylmethyl)amino>methyl>-4-nitrophenoxy>butyramide

: 116005-72-2
1-<5-<3-(N-cyclohexyl-N-methylcarbamoyl)propoxy>-2-nitrobenzyl>hydantoin

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / Ambient temperature

2: 60 percent / sodium methoxide / methanol / 18 h / Heating

With sodium methylate; triethylamine; In tetrahydrofuran; methanol;
DOI:10.1021/jm00119a015