2-butyryl-3-methoxy-4-methoxycarbonyl-5,5-dimethylcyclohex-2-en-1-one

Base Information

• Chemical Name: 2-butyryl-3-methoxy-4-methoxycarbonyl-5,5-dimethylcyclohex-2-en-1-one
• CAS No.: 118082-05-6
• Molecular Formula: C₁₅H₂₂O₅
• Molecular Weight: 282.337
• Mol file: 118082-05-6.mol

Synonyms:2-butyryl-3-methoxy-4-methoxycarbonyl-5,5-dimethylcyclohex-2-en-1-one

Chemical Property of 2-butyryl-3-methoxy-4-methoxycarbonyl-5,5-dimethylcyclohex-2-en-1-one

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 2-butyryl-3-methoxy-4-methoxycarbonyl-5,5-dimethylcyclohex-2-en-1-one

There total 1 articles about 2-butyryl-3-methoxy-4-methoxycarbonyl-5,5-dimethylcyclohex-2-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

2-butyryl-4-methoxycarbonyl-5,5-dimethylcyclohexane-1,3-dione (66421-41-8) + dimethyl sulfate (77-78-1) → 2-butyryl-3-methoxy-4-methoxycarbonyl-5,5-dimethylcyclohex-2-en-1-one (118082-05-6) + 2-butyryl-5,5-dimethyl-3-methoxy-6-methoxycarbonyl-2-cyclohexen-1-one (118082-04-5)

Guidance literature:

With sodium methylate; In acetone; for 64h; Product distribution; Ambient temperature; other reaction partner: triethylbutylammonium hydroxide; other reaction time: 48 h; other β-triketones.;

Reference yield: 98.0%

2-butyryl-3-methoxy-4-methoxycarbonyl-5,5-dimethylcyclohex-2-en-1-one (118082-05-6) → 2-butyl-5,5-dimethyl-3-methoxy-4-methoxycarbonyl-2-cyclohexen-1-one (126280-02-2)

Guidance literature:

With triethylsilane; dimethylethylsilane; In trifluoroacetic acid; for 8h; Ambient temperature;

Reference yield: 92.0%

2-butyryl-3-methoxy-4-methoxycarbonyl-5,5-dimethylcyclohex-2-en-1-one (118082-05-6) → 3-Butyryl-2-mercapto-6,6-dimethyl-4-oxo-cyclohex-2-enecarboxylic acid methyl ester

Guidance literature:

With hydrogen sulfide; sodium methylate; In methanol; for 4h; Ambient temperature;

upstream raw materials:

2-butyryl-4-methoxycarbonyl-5,5-dimethylcyclohexane-1,3-dione

dimethyl sulfate

Downstream raw materials:

2-butyl-5,5-dimethyl-3-methoxy-4-methoxycarbonyl-2-cyclohexen-1-one