(3Z,3'Z)-4,4'-(2,3,5,6-tetrafluoro-1,4-phenylene)bis{2-[4-(dimethylamino)phenyl]-1,3-butadiene-1,1,4-tricarbonitrile}

Base Information

Chemical Name:(3Z,3'Z)-4,4'-(2,3,5,6-tetrafluoro-1,4-phenylene)bis{2-[4-(dimethylamino)phenyl]-1,3-butadiene-1,1,4-tricarbonitrile}
CAS No.:1311284-45-3
Molecular Formula:C₃₆H₂₂F₄N₈
Molecular Weight:642.618
Hs Code.:

Synonyms:(3Z,3'Z)-4,4'-(2,3,5,6-tetrafluoro-1,4-phenylene)bis{2-[4-(dimethylamino)phenyl]-1,3-butadiene-1,1,4-tricarbonitrile}

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Chemical Property of (3Z,3'Z)-4,4'-(2,3,5,6-tetrafluoro-1,4-phenylene)bis{2-[4-(dimethylamino)phenyl]-1,3-butadiene-1,1,4-tricarbonitrile}

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Technology Process of (3Z,3'Z)-4,4'-(2,3,5,6-tetrafluoro-1,4-phenylene)bis{2-[4-(dimethylamino)phenyl]-1,3-butadiene-1,1,4-tricarbonitrile}

There total 3 articles about (3Z,3'Z)-4,4'-(2,3,5,6-tetrafluoro-1,4-phenylene)bis{2-[4-(dimethylamino)phenyl]-1,3-butadiene-1,1,4-tricarbonitrile} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1311284-41-9
2,2'-(2,3,5,6-tetrafluoro-1,4-phenylene)di(1,1,2-ethenetricarbonitrile)

: 17573-94-3,752235-18-0
4-ethynyl-N,N-dimethylaniline

: 1311284-45-3
(3Z,3'Z)-4,4'-(2,3,5,6-tetrafluoro-1,4-phenylene)bis{2-[4-(dimethylamino)phenyl]-1,3-butadiene-1,1,4-tricarbonitrile}

Guidance literature:: In 1,1,2,2-tetrachloroethane; at 100 ℃; for 4h; Inert atmosphere;
DOI:10.1002/chem.201003672

Reference yield:

: 3217-47-8
2,3,5,6-tetrafluoroterephthalaldehyde

: 1311284-45-3
(3Z,3'Z)-4,4'-(2,3,5,6-tetrafluoro-1,4-phenylene)bis{2-[4-(dimethylamino)phenyl]-1,3-butadiene-1,1,4-tricarbonitrile}

Guidance literature:: Multi-step reaction with 4 steps

1.1: zinc(II) chloride / 0.08 h / 100 °C / Inert atmosphere

2.1: ethanol; water / 1.25 h / 0 - 20 °C / Inert atmosphere

2.2: Inert atmosphere

3.1: N-chloro-succinimide; water / diethyl ether / 1 h / Inert atmosphere; Cooling

4.1: 1,1,2,2-tetrachloroethane / 4 h / 100 °C / Inert atmosphere

With N-chloro-succinimide; water; zinc(II) chloride; In diethyl ether; ethanol; water; 1,1,2,2-tetrachloroethane;
DOI:10.1002/chem.201003672

Reference yield:

: 1311284-40-8
C₁₄H₂F₄N₄

: 1311284-45-3
(3Z,3'Z)-4,4'-(2,3,5,6-tetrafluoro-1,4-phenylene)bis{2-[4-(dimethylamino)phenyl]-1,3-butadiene-1,1,4-tricarbonitrile}

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethanol; water / 1.25 h / 0 - 20 °C / Inert atmosphere

1.2: Inert atmosphere

2.1: N-chloro-succinimide; water / diethyl ether / 1 h / Inert atmosphere; Cooling

3.1: 1,1,2,2-tetrachloroethane / 4 h / 100 °C / Inert atmosphere

With N-chloro-succinimide; water; In diethyl ether; ethanol; water; 1,1,2,2-tetrachloroethane;
DOI:10.1002/chem.201003672