1-<(3a,4,5,6-tetrahydro-3-phenyl-3H-cyclopentisoxazol-3-yl)carbonyl>pyrrolidine

Base Information

• Chemical Name: 1-<(3a,4,5,6-tetrahydro-3-phenyl-3H-cyclopentisoxazol-3-yl)carbonyl>pyrrolidine
• CAS No.: 76504-09-1
• Molecular Formula: C₁₇H₂₀N₂O₂
• Molecular Weight: 284.358

Synonyms:1-<(3a,4,5,6-tetrahydro-3-phenyl-3H-cyclopentisoxazol-3-yl)carbonyl>pyrrolidine

Chemical Property of 1-<(3a,4,5,6-tetrahydro-3-phenyl-3H-cyclopentisoxazol-3-yl)carbonyl>pyrrolidine

Chemical Property:

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Technology Process of 1-<(3a,4,5,6-tetrahydro-3-phenyl-3H-cyclopentisoxazol-3-yl)carbonyl>pyrrolidine

There total 4 articles about 1-<(3a,4,5,6-tetrahydro-3-phenyl-3H-cyclopentisoxazol-3-yl)carbonyl>pyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4a,5,6,7-tetrahydro-4-phenyl-3-(1-pyrrolidinyl)cyclopent<1,2>oxazine 1-oxide (76504-08-0) → 1-<(3a,4,5,6-tetrahydro-3-phenyl-3H-cyclopentisoxazol-3-yl)carbonyl>pyrrolidine (76504-09-1)

Guidance literature:

In chloroform; Ambient temperature;

DOI:10.1016/S0040-4039(00)77837-3

Reference yield: 35.0%

1-nitrocyclopentene (22987-82-2) + 1-phenyl-2-(1-pyrrolidinyl)acetylene (54494-80-3) → 4a,5,6,7-tetrahydro-4-phenyl-3-(1-pyrrolidinyl)cyclopent<1,2>oxazine 1-oxide (76504-08-0) + 1-<(3a,4,5,6-tetrahydro-3-phenyl-3H-cyclopentisoxazol-3-yl)carbonyl>pyrrolidine (76504-09-1)

Guidance literature:

In Petroleum ether; Ambient temperature;

DOI:10.1016/S0040-4039(00)77837-3

Reference yield:

1-nitrocyclopentene (22987-82-2) → 1-<(3a,4,5,6-tetrahydro-3-phenyl-3H-cyclopentisoxazol-3-yl)carbonyl>pyrrolidine (76504-09-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 28 percent / petroleum ether / 24 h / 15 °C

2: 70 percent / CHCl₃ / 3 h / Heating

In chloroform; Petroleum ether;

DOI:10.1021/jo00349a004

upstream raw materials:

1-nitrocyclopentene

1-phenyl-2-(1-pyrrolidinyl)acetylene

4a,5,6,7-tetrahydro-4-phenyl-3-(1-pyrrolidinyl)cyclopent<1,2>oxazine 1-oxide

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