1-Benzyl-3-(1H-indol-3-yl)-4-{1-[2-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxy)-ethyl]-1H-indol-3-yl}-pyrrole-2,5-dione

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Chemical Name:1-Benzyl-3-(1H-indol-3-yl)-4-{1-[2-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxy)-ethyl]-1H-indol-3-yl}-pyrrole-2,5-dione
CAS No.:208777-05-3
Molecular Formula:C₄₀H₄₃N₃O₇
Molecular Weight:677.797
Hs Code.:

Synonyms:1-Benzyl-3-(1H-indol-3-yl)-4-{1-[2-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxy)-ethyl]-1H-indol-3-yl}-pyrrole-2,5-dione

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Chemical Property of 1-Benzyl-3-(1H-indol-3-yl)-4-{1-[2-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxy)-ethyl]-1H-indol-3-yl}-pyrrole-2,5-dione

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Technology Process of 1-Benzyl-3-(1H-indol-3-yl)-4-{1-[2-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxy)-ethyl]-1H-indol-3-yl}-pyrrole-2,5-dione

There total 1 articles about 1-Benzyl-3-(1H-indol-3-yl)-4-{1-[2-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxy)-ethyl]-1H-indol-3-yl}-pyrrole-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 91026-01-6
2,3-bis(1H-indol-3-yl)-N-benzylmaleimide

: 145927-73-7
2-(2-{2-[2-(2-methanesulfonyloxyethoxy)ethoxy]ethoxy}ethoxy)tetrahydro-2H-pyran

: 208777-05-3
1-Benzyl-3-(1H-indol-3-yl)-4-{1-[2-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxy)-ethyl]-1H-indol-3-yl}-pyrrole-2,5-dione

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1016/S0960-894X(98)00163-2

Reference yield:

: 208777-05-3
1-Benzyl-3-(1H-indol-3-yl)-4-{1-[2-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxy)-ethyl]-1H-indol-3-yl}-pyrrole-2,5-dione

: 1-Benzyl-3-[1-(2-{2-[2-(2-hydroxy-ethoxy)-ethoxy]-ethoxy}-ethyl)-1H-indol-3-yl]-4-(1H-indol-3-yl)-pyrrole-2,5-dione

Guidance literature:: With toluene-4-sulfonic acid; In methanol; dichloromethane;
DOI:10.1016/S0960-894X(98)00163-2

Reference yield:

: 208777-05-3
1-Benzyl-3-(1H-indol-3-yl)-4-{1-[2-(2-{2-[2-(tetrahydro-pyran-2-yloxy)-ethoxy]-ethoxy}-ethoxy)-ethyl]-1H-indol-3-yl}-pyrrole-2,5-dione

: C₆₇H₈₂N₁₀O₁₄S

Guidance literature:: Multi-step reaction with 4 steps

1: p-TsOH / CH₂Cl₂; methanol

2: 1.) 5 N KOH, 2.) AcONH₄ / 1.) EtOH, 2.) 140 deg C

3: DMAP / tetrahydrofuran

4: NaH / dimethylformamide

With dmap; potassium hydroxide; ammonium acetate; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(98)00163-2