methyl 2-(4-(cyclopent-1-en-1-yl)-3-fluorophenyl)-2,3,3,3-tetrafluoropropanoate

Base Information

Chemical Name:methyl 2-(4-(cyclopent-1-en-1-yl)-3-fluorophenyl)-2,3,3,3-tetrafluoropropanoate
CAS No.:1445076-56-1
Molecular Formula:C₁₅H₁₃F₅O₂
Molecular Weight:320.259
Hs Code.:

Synonyms:methyl 2-(4-(cyclopent-1-en-1-yl)-3-fluorophenyl)-2,3,3,3-tetrafluoropropanoate

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Chemical Property of methyl 2-(4-(cyclopent-1-en-1-yl)-3-fluorophenyl)-2,3,3,3-tetrafluoropropanoate

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Technology Process of methyl 2-(4-(cyclopent-1-en-1-yl)-3-fluorophenyl)-2,3,3,3-tetrafluoropropanoate

There total 4 articles about methyl 2-(4-(cyclopent-1-en-1-yl)-3-fluorophenyl)-2,3,3,3-tetrafluoropropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₀H₇F₅O₂

: 142-29-0
cyclopentene

: 1445076-56-1
methyl 2-(4-(cyclopent-1-en-1-yl)-3-fluorophenyl)-2,3,3,3-tetrafluoropropanoate

Guidance literature:: With palladium diacetate; In dichloromethane; at 45 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ol401558z

Reference yield:

: 1445076-24-3
(E)-methyl 2-(4-(3,3-diisopropyltriaz-1-en-1-yl)-3-fluorophenyl)-2,3,3,3-tetrafluoropropanoate

: 1445076-56-1
methyl 2-(4-(cyclopent-1-en-1-yl)-3-fluorophenyl)-2,3,3,3-tetrafluoropropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / dichloromethane / 0.33 h / 20 °C / Inert atmosphere

2: palladium diacetate / dichloromethane / 16 h / 45 °C / Inert atmosphere

With palladium diacetate; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/ol401558z

Reference yield:

: 348-54-9
2-Fluoroaniline

: 1445076-56-1
methyl 2-(4-(cyclopent-1-en-1-yl)-3-fluorophenyl)-2,3,3,3-tetrafluoropropanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: boron trifluoride diethyl etherate; isopentyl nitrite / tetrahydrofuran / 2 h / -20 °C / Inert atmosphere

1.2: 16 h / -20 - 20 °C / Inert atmosphere

2.1: silver fluoride / neat (no solvent) / 16 h / 100 °C / Inert atmosphere

3.1: trifluoroacetic acid / dichloromethane / 0.33 h / 20 °C / Inert atmosphere

4.1: palladium diacetate / dichloromethane / 16 h / 45 °C / Inert atmosphere

With boron trifluoride diethyl etherate; palladium diacetate; silver fluoride; trifluoroacetic acid; isopentyl nitrite; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol401558z