4-(4-N,N-diethylcinnamenyl)aminylbenzene

Base Information

• Chemical Name: 4-(4-N,N-diethylcinnamenyl)aminylbenzene
• CAS No.: 1202867-54-6
• Molecular Formula: C₁₈H₂₂N₂
• Molecular Weight: 266.386
• Mol file: 1202867-54-6.mol

Synonyms:4-(4-N,N-diethylcinnamenyl)aminylbenzene

Chemical Property of 4-(4-N,N-diethylcinnamenyl)aminylbenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-(4-N,N-diethylcinnamenyl)aminylbenzene

There total 3 articles about 4-(4-N,N-diethylcinnamenyl)aminylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

diethyl-(4-(4-nitro-phenylazo)-phenyl)amine (65644-11-3,17951-64-3) → 4-(4-N,N-diethylcinnamenyl)aminylbenzene (1202867-54-6)

Guidance literature:

With palladium on activated charcoal; hydrazine hydrate; In ethanol; at 80 ℃;

DOI:10.1016/j.tet.2012.05.050

Reference yield:

4-nitrobenzeneacetic acid (104-03-0) → 4-(4-N,N-diethylcinnamenyl)aminylbenzene (1202867-54-6)

Guidance literature:

Multi-step reaction with 2 steps

1: piperidine / Heating

2: tin(II) chloride dihdyrate / ethanol / 24 h / Inert atmosphere; Reflux

With piperidine; tin(II) chloride dihdyrate; In ethanol;

DOI:10.1002/cphc.201100885

Reference yield:

4-Diethylaminobenzaldehyde (120-21-8) → 4-(4-N,N-diethylcinnamenyl)aminylbenzene (1202867-54-6)

Guidance literature:

Multi-step reaction with 2 steps

1: piperidine / Heating

2: tin(II) chloride dihdyrate / ethanol / 24 h / Inert atmosphere; Reflux

With piperidine; tin(II) chloride dihdyrate; In ethanol;

DOI:10.1002/cphc.201100885

upstream raw materials:

4-nitrobenzeneacetic acid

diethyl-(4-(4-nitro-phenylazo)-phenyl)amine

4-Diethylaminobenzaldehyde

Downstream raw materials:

4-[(4'-N,N-diethylaminostilbene-4-ylimino)methyl]phenol

2-((4-(2-(4-diethylaminophenyl)vinyl)phenylimino)methyl)phenol

C₂₁H₂₁Cl₂N₅

C₃₉H₄₂ClN₇