C₃₁H₃₀N₆O₁₀

Base Information

Chemical Name:C₃₁H₃₀N₆O₁₀
CAS No.:1360804-53-0
Molecular Formula:C₃₁H₃₀N₆O₁₀
Molecular Weight:646.613
Hs Code.:

C<sub>31</sub>H<sub>30</sub>N<sub>6</sub>O<sub>10</sub>

Synonyms:C₃₁H₃₀N₆O₁₀

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Chemical Property of C₃₁H₃₀N₆O₁₀

Chemical Property:

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Technology Process of C₃₁H₃₀N₆O₁₀

There total 3 articles about C₃₁H₃₀N₆O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 621-84-1
O-benzyl carbamate

: 1360804-43-8
2-benzamido-6-chloro-9-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)purine

: 1360804-53-0
C₃₁H₃₀N₆O₁₀

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In toluene; at 85 ℃; for 5h; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.01.012

Reference yield:

: 16321-99-6
2-amino-6-chloro-9-(2,3,5-tri-O-acetyl-β-D-ribofuranosyl)purine

: 1360804-53-0
C₃₁H₃₀N₆O₁₀

Guidance literature:: Multi-step reaction with 3 steps

1: copper(l) iodide; diiodomethane; iodine; isopentyl nitrite / tetrahydrofuran

2: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / toluene / 0.67 h / 80 °C / Inert atmosphere

3: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / toluene / 5 h / 85 °C / Inert atmosphere

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; copper(l) iodide; diiodomethane; iodine; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; isopentyl nitrite; In tetrahydrofuran; toluene; 2: Buchwald-Hartwig amidation / 3: Buchwald-Hartwig amidation;
DOI:10.1016/j.tetlet.2012.01.012

Reference yield:

: 5987-76-8
6-chloro-2-iodo-9-(2',3',5'-tri-O-acetyl-β-D-ribofuranosyl)-9H-purine

: 1360804-53-0
C₃₁H₃₀N₆O₁₀

Guidance literature:: Multi-step reaction with 2 steps

1: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / 1,4-dioxane; toluene / 24 h / 0 °C / Inert atmosphere

2: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / toluene / 5 h / 85 °C / Inert atmosphere

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In 1,4-dioxane; toluene; 1: Buchwald-Hartwig amidation / 2: Buchwald-Hartwig amidation;
DOI:10.1016/j.tetlet.2012.01.012