C₂₁H₃₂N₄O₃S

Base Information

Chemical Name:C₂₁H₃₂N₄O₃S
CAS No.:1415654-87-3
Molecular Formula:C₂₁H₃₂N₄O₃S
Molecular Weight:420.576
Hs Code.:

C<sub>21</sub>H<sub>32</sub>N<sub>4</sub>O<sub>3</sub>S

Synonyms:C₂₁H₃₂N₄O₃S

Suppliers and Price of C₂₁H₃₂N₄O₃S

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₁H₃₂N₄O₃S

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₁H₃₂N₄O₃S

There total 7 articles about C₂₁H₃₂N₄O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 882491-90-9
2-((4S,5R,6S)-6-((2R,3S)-3-methoxybutan-2-yl)-2,2,5-trimethyl-1,3-dioxan-4-yl)ethanol

: 86-93-1
1-Phenyl-1H-tetrazole-5-thiol

: 1415654-87-3
C₂₁H₃₂N₄O₃S

Guidance literature:: With tributylphosphine; di-isopropyl azodicarboxylate; In tetrahydrofuran; at 0 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/jo302205t

Reference yield:

: 1415654-81-7
(R)-2-((4S,5R,6S)-6-allyl-2,2,5-trimethyl-1,3-dioxan-4-yl)-propan-1-ol

: 1415654-87-3
C₂₁H₃₂N₄O₃S

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0 °C / Inert atmosphere

2.1: tetrahydrofuran / 0 - 20 °C

3.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0 °C / Inert atmosphere

4.1: cerium(III) chloride heptahydrate; sodium tetrahydroborate / methanol / 1 h / 0 °C / Inert atmosphere

5.1: sodium hydride / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

5.2: 5 h / 20 °C

6.1: ozone / dichloromethane; methanol / -78 °C / Inert atmosphere

6.2: -78 °C

7.1: tributylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere

With sodium tetrahydroborate; tributylphosphine; cerium(III) chloride heptahydrate; di-isopropyl azodicarboxylate; sodium hydride; sodium hydrogencarbonate; Dess-Martin periodane; ozone; In tetrahydrofuran; methanol; dichloromethane; 7.1: |Mitsunobu Displacement;
DOI:10.1021/jo302205t

Reference yield:

: 955044-11-8
C₆H₁₂O₂

: 1415654-87-3
C₂₁H₃₂N₄O₃S

Guidance literature:: Multi-step reaction with 13 steps

1.1: dichloromethane / 3 h / 20 °C / Inert atmosphere

2.1: triethylamine; sodium hydrogencarbonate; water / dichloromethane / 3 h / 20 °C / pH >7

3.1: triethylamine / dichloromethane / 0 - 20 °C

4.1: sodium iodide / acetone / 24 h / Reflux

4.2: 1 h / Reflux

5.1: pyridinium p-toluenesulfonate / dichloromethane / 10 h / 20 °C

6.1: lithium; naphthalene / tetrahydrofuran / 0.5 h / -10 °C

7.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0 °C / Inert atmosphere

8.1: tetrahydrofuran / 0 - 20 °C

9.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0 °C / Inert atmosphere

10.1: cerium(III) chloride heptahydrate; sodium tetrahydroborate / methanol / 1 h / 0 °C / Inert atmosphere

11.1: sodium hydride / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

11.2: 5 h / 20 °C

12.1: ozone / dichloromethane; methanol / -78 °C / Inert atmosphere

12.2: -78 °C

13.1: tributylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere

With sodium tetrahydroborate; naphthalene; tributylphosphine; cerium(III) chloride heptahydrate; di-isopropyl azodicarboxylate; water; pyridinium p-toluenesulfonate; lithium; sodium hydride; sodium hydrogencarbonate; Dess-Martin periodane; ozone; triethylamine; sodium iodide; In tetrahydrofuran; methanol; dichloromethane; acetone; 1.1: |Prins-Kriewitz Hydroxyinethylation / 13.1: |Mitsunobu Displacement;
DOI:10.1021/jo302205t