(R)-S-ethylthio cyclohexylglycolate

Base Information

Chemical Name:(R)-S-ethylthio cyclohexylglycolate
CAS No.:157982-33-7
Molecular Formula:C₁₀H₁₈O₂S
Molecular Weight:202.318
Hs Code.:

Synonyms:(R)-S-ethylthio cyclohexylglycolate

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Chemical Property of (R)-S-ethylthio cyclohexylglycolate

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Technology Process of (R)-S-ethylthio cyclohexylglycolate

There total 4 articles about (R)-S-ethylthio cyclohexylglycolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 157982-30-4
(1R)-S-ethyl [1-cyclohexyl-1-tetrahydropyran-(2RS)-2-yloxy]thioacetate

: 157982-33-7
(R)-S-ethylthio cyclohexylglycolate

Guidance literature:: With pyridinium p-toluenesulfonate; In ethanol; at 70 ℃; for 10h;
DOI:10.1016/S0040-4020(97)01010-7

Reference yield:

: 157982-24-6
(1R,3R)-1,3-dithiane-1,3-dioxide-2-[(1R)-1-cyclohexyl]methanol

: 157982-33-7
(R)-S-ethylthio cyclohexylglycolate

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / TsOH / CH₂Cl₂

2: 1.) trifluoroacetic anhydride, pyridine, 2.) aq. LiOH / 1.) CH₂Cl₂, 0 deg C, 15 min, 2.) THF, from 0 deg C to RT

3: ethanolic PPTS

With pyridine; lithium hydroxide; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; trifluoroacetic anhydride; In dichloromethane;
DOI:10.1039/c39940001653

Reference yield:

: 2043-61-0
cyclohexanecarbaldehyde

: 157982-33-7
(R)-S-ethylthio cyclohexylglycolate

Guidance literature:: Multi-step reaction with 4 steps

1: 40 percent / NaHMDS, pyridine / tetrahydrofuran

2: 96 percent / TsOH / CH₂Cl₂

3: 1.) trifluoroacetic anhydride, pyridine, 2.) aq. LiOH / 1.) CH₂Cl₂, 0 deg C, 15 min, 2.) THF, from 0 deg C to RT

4: ethanolic PPTS

With pyridine; lithium hydroxide; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; toluene-4-sulfonic acid; trifluoroacetic anhydride; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c39940001653