Technology Process of C20H17NSi
There total 3 articles about C20H17NSi which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; tri-tert-butyl phosphine; triethylamine;
In
toluene;
for 8h;
Inert atmosphere;
DOI:10.1021/ol302922t
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 8 h / Inert atmosphere
2: copper(l) iodide; triethylamine; bis(benzonitrile)palladium(II) dichloride; tri-tert-butyl phosphine / toluene / 8 h / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; tri-tert-butyl phosphine; triethylamine;
In
toluene;
1: |Sonogashira Cross-Coupling / 2: |Sonogashira Cross-Coupling;
DOI:10.1021/ol302922t
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 8 h / Inert atmosphere
2: copper(l) iodide; triethylamine; bis(benzonitrile)palladium(II) dichloride; tri-tert-butyl phosphine / toluene / 8 h / Inert atmosphere
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; bis(benzonitrile)palladium(II) dichloride; tri-tert-butyl phosphine; triethylamine;
In
toluene;
1: |Sonogashira Cross-Coupling / 2: |Sonogashira Cross-Coupling;
DOI:10.1021/ol302922t