C₃₅H₄₉N₃O₉

Base Information

Chemical Name:C₃₅H₄₉N₃O₉
CAS No.:1255213-49-0
Molecular Formula:C₃₅H₄₉N₃O₉
Molecular Weight:655.789
Hs Code.:

C<sub>35</sub>H<sub>49</sub>N<sub>3</sub>O<sub>9</sub>

Synonyms:C₃₅H₄₉N₃O₉

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Chemical Property of C₃₅H₄₉N₃O₉

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Technology Process of C₃₅H₄₉N₃O₉

There total 16 articles about C₃₅H₄₉N₃O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1255213-41-2
C₃₇H₅₃N₃O₉

: 1255213-49-0
C₃₅H₄₉N₃O₉

Guidance literature:: With Hoveyda-Grubbs catalyst second generation; p-benzoquinone; In toluene; at 40 ℃; for 14h; Inert atmosphere;
DOI:10.1021/ja105119r

Reference yield:

: 1255213-20-7
(R)-methyl 5-nitro-2-(pent-4-en-2-yloxy)benzoate

: 1255213-49-0
C₃₅H₄₉N₃O₉

Guidance literature:: Multi-step reaction with 5 steps

1.1: water; sodium hydroxide / tetrahydrofuran; methanol / 23 h

1.2: pH 1

2.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 14 h / 0 - 20 °C

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 14 h / 0 - 20 °C

5.1: Hoveyda-Grubbs catalyst second generation; p-benzoquinone / toluene / 14 h / 40 °C / Inert atmosphere

With Hoveyda-Grubbs catalyst second generation; tetrabutyl ammonium fluoride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; water; sodium hydride; N-ethyl-N,N-diisopropylamine; p-benzoquinone; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil;
DOI:10.1021/ja105119r

Reference yield:

: 1255214-43-7
(R)-5-nitro-2-(pent-4-en-2-yloxy)benzoic acid

: 1255213-49-0
C₃₅H₄₉N₃O₉

Guidance literature:: Multi-step reaction with 4 steps

1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 14 h / 0 - 20 °C

3: sodium hydride / N,N-dimethyl-formamide; mineral oil / 14 h / 0 - 20 °C

4: Hoveyda-Grubbs catalyst second generation; p-benzoquinone / toluene / 14 h / 40 °C / Inert atmosphere

With Hoveyda-Grubbs catalyst second generation; tetrabutyl ammonium fluoride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; sodium hydride; N-ethyl-N,N-diisopropylamine; p-benzoquinone; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; toluene; mineral oil;
DOI:10.1021/ja105119r