tert-butyl 2-(benzyloxycarbonylamino)-2-(3-(tert-butyldimethylsilyloxy)propyl)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanoate

Base Information

Chemical Name:tert-butyl 2-(benzyloxycarbonylamino)-2-(3-(tert-butyldimethylsilyloxy)propyl)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanoate
CAS No.:1384298-49-0
Molecular Formula:C₃₃H₅₈BNO₇Si
Molecular Weight:619.723
Hs Code.:

Synonyms:tert-butyl 2-(benzyloxycarbonylamino)-2-(3-(tert-butyldimethylsilyloxy)propyl)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanoate

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Chemical Property of tert-butyl 2-(benzyloxycarbonylamino)-2-(3-(tert-butyldimethylsilyloxy)propyl)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanoate

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Technology Process of tert-butyl 2-(benzyloxycarbonylamino)-2-(3-(tert-butyldimethylsilyloxy)propyl)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanoate

There total 1 articles about tert-butyl 2-(benzyloxycarbonylamino)-2-(3-(tert-butyldimethylsilyloxy)propyl)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1384298-49-0
tert-butyl 2-(benzyloxycarbonylamino)-2-(3-(tert-butyldimethylsilyloxy)propyl)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanoate

Guidance literature:

Reference yield:

: 1384298-49-0
tert-butyl 2-(benzyloxycarbonylamino)-2-(3-(tert-butyldimethylsilyloxy)propyl)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanoate

: 1384298-58-1
C₂₇H₄₄BNO₇

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃; Inert atmosphere;

Reference yield:

: 1384298-49-0
tert-butyl 2-(benzyloxycarbonylamino)-2-(3-(tert-butyldimethylsilyloxy)propyl)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanoate

: 1384298-75-2
tert-butyl 2-(benzyloxylcarbonylamino)-2-(3-(3-phenylpiperidin-1-yl)propyl)-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)hexanoate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / water; tetrahydrofuran / 20 °C / Inert atmosphere

2: 1H-imidazole; iodine / Ph₃P-resin / dichloromethane / 20 °C / Inert atmosphere

3: potassium carbonate / N,N-dimethyl-formamide / 20 °C

With 1H-imidazole; hydrogenchloride; iodine; potassium carbonate; Ph₃P-resin; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;