(E)-N,N'-(4-phenylbut-3-ene-1,2-diyl)dimethanesulfonamide

Base Information

Chemical Name:(E)-N,N'-(4-phenylbut-3-ene-1,2-diyl)dimethanesulfonamide
CAS No.:1379606-39-9
Molecular Formula:C₁₂H₁₈N₂O₄S₂
Molecular Weight:318.418
Hs Code.:

Synonyms:(E)-N,N'-(4-phenylbut-3-ene-1,2-diyl)dimethanesulfonamide

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Chemical Property of (E)-N,N'-(4-phenylbut-3-ene-1,2-diyl)dimethanesulfonamide

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Technology Process of (E)-N,N'-(4-phenylbut-3-ene-1,2-diyl)dimethanesulfonamide

There total 4 articles about (E)-N,N'-(4-phenylbut-3-ene-1,2-diyl)dimethanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1379605-98-7
(E)-N,N'-(4-phenylbut-3-ene-1,2-diyl)bis(N-(methylsulfonyl)methanesulfonamide)

: 1379606-39-9
(E)-N,N'-(4-phenylbut-3-ene-1,2-diyl)dimethanesulfonamide

Guidance literature:: (E)-N,N'-(4-phenylbut-3-ene-1,2-diyl)bis(N-(methylsulfonyl)methanesulfonamide); With potassium hydroxide; In tetrahydrofuran; at 20 ℃; for 18h;

With hydrogenchloride; In tetrahydrofuran; water; at 0 ℃;
DOI:10.1002/chem.201103435

Reference yield:

: 14371-10-9
(E)-3-phenylpropenal

: 1379606-39-9
(E)-N,N'-(4-phenylbut-3-ene-1,2-diyl)dimethanesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; cyclohexane / 0.25 h / 0 °C

1.2: 2 h / 0 - 20 °C

2.1: dichloromethane / 0.08 h / 20 °C

2.2: 12 h / 20 °C

3.1: potassium hydroxide / tetrahydrofuran / 18 h / 20 °C

3.2: 0 °C

With n-butyllithium; potassium hydroxide; In tetrahydrofuran; dichloromethane; cyclohexane; 1.2: Wittig olefination;
DOI:10.1002/chem.201103435

Reference yield:

: 16939-57-4
(E)-buta-1,3-dienylbenzene

: 1379606-39-9
(E)-N,N'-(4-phenylbut-3-ene-1,2-diyl)dimethanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 0.08 h / 20 °C

1.2: 12 h / 20 °C

2.1: potassium hydroxide / tetrahydrofuran / 18 h / 20 °C

2.2: 0 °C

With potassium hydroxide; In tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.201103435