benzyl (6-benzyloxycarbonylaminohexyl) 2,6-O-bis(benzyloxymethyl)-D-myo-insit-1-yl phosphate 3,4,5-tris(dibenzyl phosphate)

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Chemical Name:benzyl (6-benzyloxycarbonylaminohexyl) 2,6-O-bis(benzyloxymethyl)-D-myo-insit-1-yl phosphate 3,4,5-tris(dibenzyl phosphate)
CAS No.:1188371-77-8
Molecular Formula:C₈₅H₉₃NO₂₂P₄
Molecular Weight:1604.56
Hs Code.:

Synonyms:benzyl (6-benzyloxycarbonylaminohexyl) 2,6-O-bis(benzyloxymethyl)-D-myo-insit-1-yl phosphate 3,4,5-tris(dibenzyl phosphate)

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Chemical Property of benzyl (6-benzyloxycarbonylaminohexyl) 2,6-O-bis(benzyloxymethyl)-D-myo-insit-1-yl phosphate 3,4,5-tris(dibenzyl phosphate)

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Technology Process of benzyl (6-benzyloxycarbonylaminohexyl) 2,6-O-bis(benzyloxymethyl)-D-myo-insit-1-yl phosphate 3,4,5-tris(dibenzyl phosphate)

There total 1 articles about benzyl (6-benzyloxycarbonylaminohexyl) 2,6-O-bis(benzyloxymethyl)-D-myo-insit-1-yl phosphate 3,4,5-tris(dibenzyl phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: benzyl N-Cbz-6-aminohexyl diisopropylphosphoramidite

: 163563-70-0
2,6-Bis-O-<(benzyloxy)methyl>-3,4,5-tris-O-(dibenzylphosphoryl)-D-myo-inositol

: 1188371-77-8
benzyl (6-benzyloxycarbonylaminohexyl) 2,6-O-bis(benzyloxymethyl)-D-myo-insit-1-yl phosphate 3,4,5-tris(dibenzyl phosphate)

Guidance literature:: benzyl N-Cbz-6-aminohexyl diisopropylphosphoramidite; 2,6-Bis-O-<(benzyloxy)methyl>-3,4,5-tris-O-(dibenzylphosphoryl)-D-myo-inositol; With 1H-tetrazole; In dichloromethane; acetonitrile; at 20 ℃; for 18h; Inert atmosphere;

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetonitrile; at -60 - 20 ℃;
DOI:10.1002/ejoc.200900476

Reference yield: 100.0%

: 1188371-77-8
benzyl (6-benzyloxycarbonylaminohexyl) 2,6-O-bis(benzyloxymethyl)-D-myo-insit-1-yl phosphate 3,4,5-tris(dibenzyl phosphate)

: 1-(6-aminohexyl sodium phosphate)-D-myo-insitol 3,4,5-tris(disodium phosphate)

Guidance literature:: benzyl (6-benzyloxycarbonylaminohexyl) 2,6-O-bis(benzyloxymethyl)-D-myo-insit-1-yl phosphate 3,4,5-tris(dibenzyl phosphate); With Pearlman catalyst; hydrogen; In methanol; at 20 ℃; for 72h; under 760.051 Torr;

In water; for 3h;
DOI:10.1002/ejoc.200900476