2,3-bis(2-cyanoethylthio)-6,7-bis(3,5-di-tert-butylbenzylthio)-1,4,5,8-tetrathiafulvalene

Base Information

Chemical Name:2,3-bis(2-cyanoethylthio)-6,7-bis(3,5-di-tert-butylbenzylthio)-1,4,5,8-tetrathiafulvalene
CAS No.:1204138-61-3
Molecular Formula:C₄₂H₅₄N₂S₈
Molecular Weight:843.432
Hs Code.:

Synonyms:2,3-bis(2-cyanoethylthio)-6,7-bis(3,5-di-tert-butylbenzylthio)-1,4,5,8-tetrathiafulvalene

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Chemical Property of 2,3-bis(2-cyanoethylthio)-6,7-bis(3,5-di-tert-butylbenzylthio)-1,4,5,8-tetrathiafulvalene

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MSDS Files:: SDS file from LookChem

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Technology Process of 2,3-bis(2-cyanoethylthio)-6,7-bis(3,5-di-tert-butylbenzylthio)-1,4,5,8-tetrathiafulvalene

There total 1 articles about 2,3-bis(2-cyanoethylthio)-6,7-bis(3,5-di-tert-butylbenzylthio)-1,4,5,8-tetrathiafulvalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 1204138-60-2
4,5-bis(3,5-di-tert-butylbenzylthio)-1,3-dithiole-2-thione

: 158871-28-4
4,5-bis(2-cyanoethylthio)-1,3-dithiol-2-one

: 1204138-61-3
2,3-bis(2-cyanoethylthio)-6,7-bis(3,5-di-tert-butylbenzylthio)-1,4,5,8-tetrathiafulvalene

: 132765-36-7
2,3,6,7-tetrakis(2-cyanoethylthio)tetrathiafulvalene

Guidance literature:: With triethyl phosphite; at 120 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tet.2009.10.052

Reference yield: 81.0%

: 1204138-61-3
2,3-bis(2-cyanoethylthio)-6,7-bis(3,5-di-tert-butylbenzylthio)-1,4,5,8-tetrathiafulvalene

: 139200-74-1
2,3-bis(bromomethyl)-1,4-dihexyloxybenzene

: 1204138-66-8
2-[4,5-bis(3,5-di-tert-butylbenzylthio)-1,3-dithiol-2-ylidene]-5H,10H-6,9-dihexyloxy-1,3-dithiolo[4,5-c][2,5]benzodithiocine

Guidance literature:: 2,3-bis(2-cyanoethylthio)-6,7-bis(3,5-di-tert-butylbenzylthio)-1,4,5,8-tetrathiafulvalene; With cesium hydroxide; In methanol; N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;

2,3-bis(bromomethyl)-1,4-dihexyloxybenzene; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; at -20 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2009.10.052

Reference yield: 77.0%

: 1204138-61-3
2,3-bis(2-cyanoethylthio)-6,7-bis(3,5-di-tert-butylbenzylthio)-1,4,5,8-tetrathiafulvalene

: 88903-14-4
2,3,6,7-tetrakis(bromomethyl)naphthalene

: 1204138-68-0
C₈₆H₁₀₄S₁₆

Guidance literature:: 2,3-bis(2-cyanoethylthio)-6,7-bis(3,5-di-tert-butylbenzylthio)-1,4,5,8-tetrathiafulvalene; With cesium hydroxide; In methanol; N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;

2,3,6,7-tetrakis(bromomethyl)naphthalene; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; at -20 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2009.10.052