1-O-(glycylglycyl-L-phenylalanyl)-β-D-glucopyranose trifluoroacetate

Base Information

Chemical Name:1-O-(glycylglycyl-L-phenylalanyl)-β-D-glucopyranose trifluoroacetate
CAS No.:75720-14-8
Molecular Formula:C₂HF₃O₂*C₁₉H₂₇N₃O₉
Molecular Weight:555.462
Hs Code.:

Synonyms:1-O-(glycylglycyl-L-phenylalanyl)-β-D-glucopyranose trifluoroacetate

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Chemical Property of 1-O-(glycylglycyl-L-phenylalanyl)-β-D-glucopyranose trifluoroacetate

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Technology Process of 1-O-(glycylglycyl-L-phenylalanyl)-β-D-glucopyranose trifluoroacetate

There total 6 articles about 1-O-(glycylglycyl-L-phenylalanyl)-β-D-glucopyranose trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 75719-92-5
2,3,4,6-tetra-O-benzyl-1-O-(N-benzyloxycarbonylglycylglycyl-L-phenylalanyl)-β-D-glucopyranose

: 76-05-1
trifluoroacetic acid

: 75720-14-8
1-O-(glycylglycyl-L-phenylalanyl)-β-D-glucopyranose trifluoroacetate

Guidance literature:: With hydrogen; palladium on activated charcoal; In 2-methoxy-ethanol; acetic acid; for 24h;
DOI:10.1016/S0008-6215(00)85517-2

Reference yield: 61.0%

: 75719-90-3,75719-91-4,75719-92-5,75719-93-6
2,3,4,6-tetra-O-benzyl-1-O-(N-benzyloxycarbonylglycylglycyl-L,D-phenylalanyl)-α-D-glucopyranose

: 76-05-1
trifluoroacetic acid

: 75720-14-8,75720-18-2
1-O-(glycylglycyl-L-phenylalanyl)-α-D-glucopyranose trifluoroacetate

Guidance literature:: With hydrogen; palladium on activated charcoal; In 2-methoxy-ethanol; for 20h;
DOI:10.1016/S0008-6215(00)85517-2

Reference yield:

: 6233-98-3
N-benzyloxycarbonyl-glycylglycyl-L-phenylalanine pentachlorophenyl ester

: 75720-14-8,75720-18-2
1-O-(glycylglycyl-L-phenylalanyl)-α-D-glucopyranose trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: imidazole / dimethylformamide / 48 h / Ambient temperature

2: 61 percent / H₂ / 10percent Pd/C / 2-methoxy-ethanol / 20 h

With 1H-imidazole; hydrogen; palladium on activated charcoal; In 2-methoxy-ethanol; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)85517-2