WBr(NNH₂)(NC₅H₅)(P(CH₃)2C₆H₅)3⁽¹⁺⁾*Br^(1-)=[WBr(NNH₂)(NC₅H₅)(P(CH₃)2C₆H₅)3]Br

Base Information

Chemical Name:WBr(NNH₂)(NC₅H₅)(P(CH₃)2C₆H₅)3⁽¹⁺⁾*Br^(1-)=[WBr(NNH₂)(NC₅H₅)(P(CH₃)2C₆H₅)3]Br
CAS No.:69569-15-9
Molecular Formula:Br*C₂₉H₄₀BrN₃P₃W
Molecular Weight:867.236
Hs Code.:

WBr(NNH<sub>2</sub>)(NC<sub>5</sub>H<sub>5</sub>)(P(CH<sub>3</sub>)2C<sub>6</sub>H<sub>5</sub>)3<sup>(1+)</sup>*Br<sup>(1-)</sup>=[WBr(NNH<sub>2</sub>)(NC<sub>5</sub>H<sub>5</sub>)(P(CH<sub>3</sub>)2C<sub>6</sub>H<sub>5</sub>)3]Br

Synonyms:WBr(NNH₂)(NC₅H₅)(P(CH₃)2C₆H₅)3⁽¹⁺⁾*Br^(1-)=[WBr(NNH₂)(NC₅H₅)(P(CH₃)2C₆H₅)3]Br

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Chemical Property of WBr(NNH₂)(NC₅H₅)(P(CH₃)2C₆H₅)3⁽¹⁺⁾*Br^(1-)=[WBr(NNH₂)(NC₅H₅)(P(CH₃)2C₆H₅)3]Br

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Technology Process of WBr(NNH₂)(NC₅H₅)(P(CH₃)2C₆H₅)3⁽¹⁺⁾*Br^(1-)=[WBr(NNH₂)(NC₅H₅)(P(CH₃)2C₆H₅)3]Br

There total 1 articles about WBr(NNH₂)(NC₅H₅)(P(CH₃)2C₆H₅)3⁽¹⁺⁾*Br^(1-)=[WBr(NNH₂)(NC₅H₅)(P(CH₃)2C₆H₅)3]Br which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 58081-44-0,69610-32-8
dibromotris(dimethylphenylphosphine)[hydrazido^(2-)]tungsten(IV)

: 69569-15-9
WBr(NNH₂)(NC₅H₅)(P(CH₃)2C₆H₅)3⁽¹⁺⁾*Br^(1-)=[WBr(NNH₂)(NC₅H₅)(P(CH₃)2C₆H₅)3]Br

Guidance literature:: With pyridine; In pyridine; N2-atmosphere; dissoln. of W-complex; crystn. on Et2O addn.; elem. anal.;
DOI:10.1039/DT9780001766

Reference yield: 71.0%

: 69569-15-9
WBr(NNH₂)(NC₅H₅)(P(CH₃)2C₆H₅)3⁽¹⁺⁾*Br^(1-)=[WBr(NNH₂)(NC₅H₅)(P(CH₃)2C₆H₅)3]Br

: 143-66-8
sodium tetraphenyl borate

: 69569-28-4
WBr(NNH₂)(NC₅H₅)(P(CH₃)2C₆H₅)3⁽¹⁺⁾*B(C₆H₅)4^(1-)=[WBr(NNH₂)(NC₅H₅)(P(CH₃ )2C₆H₅)3][B(C₆H₅)4]

Guidance literature:: In tetrahydrofuran; dichloromethane; addn. of solvents to mixt. of W-complex and NaBPh4, dissoln. on stirring(N2-atmosphere, 20°C); filtration, evapn., extn. into CH2Cl2, crystn. on Et2O addn.; elem. anal.;
DOI:10.1039/DT9780001766