2-(4-hydroxymethyl-3-nitrophenyl)-2,5,5-trimethylpyrrolidin-1-yloxy radical

Base Information

Chemical Name:2-(4-hydroxymethyl-3-nitrophenyl)-2,5,5-trimethylpyrrolidin-1-yloxy radical
CAS No.:791100-85-1
Molecular Formula:C₁₄H₁₉N₂O₄
Molecular Weight:279.316
Hs Code.:

Synonyms:2-(4-hydroxymethyl-3-nitrophenyl)-2,5,5-trimethylpyrrolidin-1-yloxy radical

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Chemical Property of 2-(4-hydroxymethyl-3-nitrophenyl)-2,5,5-trimethylpyrrolidin-1-yloxy radical

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Technology Process of 2-(4-hydroxymethyl-3-nitrophenyl)-2,5,5-trimethylpyrrolidin-1-yloxy radical

There total 4 articles about 2-(4-hydroxymethyl-3-nitrophenyl)-2,5,5-trimethylpyrrolidin-1-yloxy radical which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₂₁N₂O₅

: 791100-85-1
2-(4-hydroxymethyl-3-nitrophenyl)-2,5,5-trimethylpyrrolidin-1-yloxy radical

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 0.5h;
DOI:10.1055/s-2004-829172

Reference yield:

: 328000-35-7
2-(4-Hydroxymethylphenyl)-2,5,5-trimethylpyrrolidin-1-yloxyl radical

: 791100-85-1
2-(4-hydroxymethyl-3-nitrophenyl)-2,5,5-trimethylpyrrolidin-1-yloxy radical

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / Et₃N / CH₂Cl₂ / 0 - 20 °C

2: HNO₃; H₂SO₄ / 3 h / 0 °C

3: 1.75 g / NaOMe / methanol / 0.5 h / 20 °C

With sulfuric acid; nitric acid; sodium methylate; triethylamine; In methanol; dichloromethane;
DOI:10.1055/s-2004-829172

Reference yield:

: 328000-34-6
4-(1-Oxyl-2,5,5-trimethylpyrrolidin-2-yl)benzaldehyde radical

: 791100-85-1
2-(4-hydroxymethyl-3-nitrophenyl)-2,5,5-trimethylpyrrolidin-1-yloxy radical

Guidance literature:: Multi-step reaction with 4 steps

1: 72 percent / NaBH₄ / ethanol / 20 °C

2: 75 percent / Et₃N / CH₂Cl₂ / 0 - 20 °C

3: HNO₃; H₂SO₄ / 3 h / 0 °C

4: 1.75 g / NaOMe / methanol / 0.5 h / 20 °C

With sodium tetrahydroborate; sulfuric acid; nitric acid; sodium methylate; triethylamine; In methanol; ethanol; dichloromethane;
DOI:10.1055/s-2004-829172