{(1R,2R,3S,5R)-2-[(α-L-fucopyranosyl)oxy]-3,5-dimethylcyclohex-1-yl} 3-O-[sodium (1S)-1-carboxy-2-cyclohexylethyl]-β-D-galactopyranoside

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Chemical Name:{(1R,2R,3S,5R)-2-[(α-L-fucopyranosyl)oxy]-3,5-dimethylcyclohex-1-yl} 3-O-[sodium (1S)-1-carboxy-2-cyclohexylethyl]-β-D-galactopyranoside
CAS No.:1361093-44-8
Molecular Formula:C₂₉H₄₉O₁₃*Na
Molecular Weight:628.69
Hs Code.:

Synonyms:{(1R,2R,3S,5R)-2-[(α-L-fucopyranosyl)oxy]-3,5-dimethylcyclohex-1-yl} 3-O-[sodium (1S)-1-carboxy-2-cyclohexylethyl]-β-D-galactopyranoside

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Chemical Property of {(1R,2R,3S,5R)-2-[(α-L-fucopyranosyl)oxy]-3,5-dimethylcyclohex-1-yl} 3-O-[sodium (1S)-1-carboxy-2-cyclohexylethyl]-β-D-galactopyranoside

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Technology Process of {(1R,2R,3S,5R)-2-[(α-L-fucopyranosyl)oxy]-3,5-dimethylcyclohex-1-yl} 3-O-[sodium (1S)-1-carboxy-2-cyclohexylethyl]-β-D-galactopyranoside

There total 2 articles about {(1R,2R,3S,5R)-2-[(α-L-fucopyranosyl)oxy]-3,5-dimethylcyclohex-1-yl} 3-O-[sodium (1S)-1-carboxy-2-cyclohexylethyl]-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1026074-38-3
{(1R,2R,3S,5R)-2-[(α-L-fucopyranosyl)oxy]-3,5-dimethylcyclohex-1-yl} 2-O-benzoyl-3-O-[sodium (1S)-1-carboxy-2-cyclohexylethyl]-β-D-galactopyranoside

: 1361093-44-8
{(1R,2R,3S,5R)-2-[(α-L-fucopyranosyl)oxy]-3,5-dimethylcyclohex-1-yl} 3-O-[sodium (1S)-1-carboxy-2-cyclohexylethyl]-β-D-galactopyranoside

Guidance literature:: {(1R,2R,3S,5R)-2-[(α-L-fucopyranosyl)oxy]-3,5-dimethylcyclohex-1-yl} 2-O-benzoyl-3-O-[sodium (1S)-1-carboxy-2-cyclohexylethyl]-β-D-galactopyranoside; With lithium hydroxide; In methanol; water; at 20 ℃; for 18h;

In methanol; water;
DOI:10.1002/chem.201102884

Reference yield:

: C₅₇H₆₈O₁₆

: 1361093-44-8
{(1R,2R,3S,5R)-2-[(α-L-fucopyranosyl)oxy]-3,5-dimethylcyclohex-1-yl} 3-O-[sodium (1S)-1-carboxy-2-cyclohexylethyl]-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium methylate / methanol / 16 h / 20 °C

2.1: lithium hydroxide / methanol; water / 18 h / 20 °C

2.2: Dowex 50X₈ (Na+ form)

With sodium methylate; lithium hydroxide; In methanol; water;
DOI:10.1002/chem.201102884