2-<(methylsulfinyl)methyl>-6-<(methylthio)methyl>phenyl phenyl sulfoxide

Base Information

Chemical Name:2-<(methylsulfinyl)methyl>-6-<(methylthio)methyl>phenyl phenyl sulfoxide
CAS No.:108428-24-6
Molecular Formula:C₁₆H₁₈OS₃
Molecular Weight:322.516
Hs Code.:

Synonyms:2-<(methylsulfinyl)methyl>-6-<(methylthio)methyl>phenyl phenyl sulfoxide

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Chemical Property of 2-<(methylsulfinyl)methyl>-6-<(methylthio)methyl>phenyl phenyl sulfoxide

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Technology Process of 2-<(methylsulfinyl)methyl>-6-<(methylthio)methyl>phenyl phenyl sulfoxide

There total 8 articles about 2-<(methylsulfinyl)methyl>-6-<(methylthio)methyl>phenyl phenyl sulfoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 112399-12-9
2,6-bis(bromomethyl) phenyl phenyl sulphide

: 108428-24-6
2-<(methylsulfinyl)methyl>-6-<(methylthio)methyl>phenyl phenyl sulfoxide

Guidance literature:: Multi-step reaction with 2 steps

2: sodium metaperiodate

With sodium periodate;
DOI:10.1039/c39860001359

Reference yield:

: 108428-22-4
2,6-bis<(methylthio)methyl>phenyl phenyl sulfide

: 108428-24-6
2-<(methylsulfinyl)methyl>-6-<(methylthio)methyl>phenyl phenyl sulfoxide

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 3h; Ambient temperature;
DOI:10.1021/ja00212a042

Reference yield:

: 118-72-9
2,6-dimethylbenzene-1-thiol

: 108428-24-6
2-<(methylsulfinyl)methyl>-6-<(methylthio)methyl>phenyl phenyl sulfoxide

Guidance literature:: Multi-step reaction with 4 steps

1: 60percent sodium hydride, CuI / hexamethylphosphoric acid triamide / 17 h / 105 °C

2: N-bromosuccinimide / CCl₄ / 46 h / 15 °C / Irradiation

3: 81 percent / tetrabutylammonium bromide / benzene; H₂O / 12 h / 50 °C

4: 85percent m-chloroperbenzoic acid / CH₂Cl₂ / 3 h / Ambient temperature

With N-Bromosuccinimide; copper(l) iodide; tetrabutylammomium bromide; sodium hydride; 3-chloro-benzenecarboperoxoic acid; In tetrachloromethane; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane; water; benzene;
DOI:10.1021/ja00212a042