7-cyclopropyl-6-(4-methoxyphenyl)-3-tosyl-3-azabicyclo[4.1.0]hept-4-ene

Base Information

• Chemical Name: 7-cyclopropyl-6-(4-methoxyphenyl)-3-tosyl-3-azabicyclo[4.1.0]hept-4-ene
• CAS No.: 1233490-13-5
• Molecular Formula: C₂₃H₂₅NO₃S
• Molecular Weight: 395.522

Synonyms:7-cyclopropyl-6-(4-methoxyphenyl)-3-tosyl-3-azabicyclo[4.1.0]hept-4-ene

Chemical Property of 7-cyclopropyl-6-(4-methoxyphenyl)-3-tosyl-3-azabicyclo[4.1.0]hept-4-ene

Chemical Property:

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Technology Process of 7-cyclopropyl-6-(4-methoxyphenyl)-3-tosyl-3-azabicyclo[4.1.0]hept-4-ene

There total 1 articles about 7-cyclopropyl-6-(4-methoxyphenyl)-3-tosyl-3-azabicyclo[4.1.0]hept-4-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C23H25NO3S (1194434-86-0) → 7-cyclopropyl-6-(4-methoxyphenyl)-3-tosyl-3-azabicyclo[4.1.0]hept-4-ene (1233490-13-5)

Guidance literature:

With platinum(II) chloride; In toluene; at 80 ℃; Inert atmosphere;

DOI:10.1002/chem.200902284

Reference yield: 76.0%

7-cyclopropyl-6-(4-methoxyphenyl)-3-tosyl-3-azabicyclo[4.1.0]hept-4-ene (1233490-13-5) → 8-(4-methoxyphenyl)-4-methyl-6-tosyl-6-azabicyclo[3.2.2]nona-2,8-diene

Guidance literature:

With silver hexafluoroantimonate; trans-carbonyl(chloro)bis(triphenylphosphine)rhodium(I); In 1,4-dioxane; at 20 ℃; for 0.0833333h; Inert atmosphere;

7-cyclopropyl-6-(4-methoxyphenyl)-3-tosyl-3-azabicyclo[4.1.0]hept-4-ene; In 1,4-dioxane; at 100 ℃; for 18h; Inert atmosphere;

DOI:10.1002/chem.200902284

upstream raw materials:

C₂₃H₂₅NO₃S

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