tert-butyl (E)-4-benzyloxybut-2-enyl carbonate

Base Information

Chemical Name:tert-butyl (E)-4-benzyloxybut-2-enyl carbonate
CAS No.:1169852-11-2
Molecular Formula:C₁₆H₂₂O₄
Molecular Weight:278.348
Hs Code.:

Synonyms:tert-butyl (E)-4-benzyloxybut-2-enyl carbonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyl (E)-4-benzyloxybut-2-enyl carbonate

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Technology Process of tert-butyl (E)-4-benzyloxybut-2-enyl carbonate

There total 1 articles about tert-butyl (E)-4-benzyloxybut-2-enyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 80885-30-9,81028-03-7,69152-88-1
(E)-4-(benzyloxy)-2-buten-1-ol

: 1169852-11-2
tert-butyl (E)-4-benzyloxybut-2-enyl carbonate

Guidance literature:: With tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide; In dichloromethane; water;
DOI:10.1021/ol901151u

Reference yield: 70.0%

: 3770-50-1,117770-52-2
2-carbethoxyindole

: 1169852-11-2
tert-butyl (E)-4-benzyloxybut-2-enyl carbonate

: 1198150-85-4
C₂₂H₂₃NO₃

: 1198150-80-9
(R)-ethyl 1-(1-(benzyloxy)but-3-en-2-yl)-1H-indole-2-carboxylate

Guidance literature:: With [Ir(cod)(κ2-(Ra,Rc,Rc)-(C10H6)2O2PN(CHCH2(2-MeOC6H)4)2H(ethylene)]; caesium carbonate; In tetrahydrofuran; at 20 ℃; for 6h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1002/anie.200904338

Reference yield: 65.0%

: 4248-19-5
tert-butyl carbazate

: 1169852-11-2
tert-butyl (E)-4-benzyloxybut-2-enyl carbonate

: 1242146-15-1
tert-butyl {(1S)-1-[(benzyloxy)methyl]prop-2-enyl}carbamate

Guidance literature:: With C₄₈H₄₇IrNO₄P; In diethyl ether; at 20 ℃; for 21h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ol901151u