bis-cyanoethyl [1-chloro-5-{1-(2,2,2-trifluoroethoxy-5'-chlorotricyclo[3.3.1.1.^3,7]dec-2-ylidenemethyl)}]phenylphosphate

Base Information

• Chemical Name: bis-cyanoethyl [1-chloro-5-{1-(2,2,2-trifluoroethoxy-5'-chlorotricyclo[3.3.1.1.^3,7]dec-2-ylidenemethyl)}]phenylphosphate
• CAS No.: 882429-24-5
• Molecular Formula: C₂₅H₂₆Cl₂F₃N₂O₅P
• Molecular Weight: 593.367

Synonyms:bis-cyanoethyl [1-chloro-5-{1-(2,2,2-trifluoroethoxy-5'-chlorotricyclo[3.3.1.1.^3,7]dec-2-ylidenemethyl)}]phenylphosphate

Chemical Property of bis-cyanoethyl [1-chloro-5-{1-(2,2,2-trifluoroethoxy-5'-chlorotricyclo[3.3.1.1.^3,7]dec-2-ylidenemethyl)}]phenylphosphate

Chemical Property:

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Technology Process of bis-cyanoethyl [1-chloro-5-{1-(2,2,2-trifluoroethoxy-5'-chlorotricyclo[3.3.1.1.^3,7]dec-2-ylidenemethyl)}]phenylphosphate

There total 1 articles about bis-cyanoethyl [1-chloro-5-{1-(2,2,2-trifluoroethoxy-5'-chlorotricyclo[3.3.1.1.^3,7]dec-2-ylidenemethyl)}]phenylphosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.6%

2-chloro-5-{1-(2,2,2-trifluoroethoxy-5'-chloro-tricyclo[3.3.1.13,7]dec-2-ylidenemethyl)}phenol (189942-79-8) + 3-Hydroxypropionitrile (109-78-4) → bis-cyanoethyl [1-chloro-5-{1-(2,2,2-trifluoroethoxy-5'-chlorotricyclo[3.3.1.1.3,7]dec-2-ylidenemethyl)}]phenylphosphate (882429-24-5)

Guidance literature:

2-chloro-5-{1-(2,2,2-trifluoroethoxy-5'-chloro-tricyclo[3.3.1.1^3,7]dec-2-ylidenemethyl)}phenol; With pyridine; trichlorophosphate; In tetrahydrofuran; at 0 - 20 ℃; for 4.86667h;

3-Hydroxypropionitrile; In tetrahydrofuran; at 0 - 20 ℃; for 66.0833h;

Reference yield:

bis-cyanoethyl [1-chloro-5-{1-(2,2,2-trifluoroethoxy-5'-chlorotricyclo[3.3.1.1.3,7]dec-2-ylidenemethyl)}]phenylphosphate (882429-24-5) → C25H26Cl2F3N2O7P

Guidance literature:

bis-cyanoethyl [1-chloro-5-{1-(2,2,2-trifluoroethoxy-5'-chlorotricyclo[3.3.1.1.^3,7]dec-2-ylidenemethyl)}]phenylphosphate; With 5,15,10,20-tetraphenylporphyrin; In methanol; chloroform; at 20 ℃; for 0.5h;

With oxygen; In chloroform; at 0 ℃; for 12h; UV-irradiation;

Reference yield:

bis-cyanoethyl [1-chloro-5-{1-(2,2,2-trifluoroethoxy-5'-chlorotricyclo[3.3.1.1.3,7]dec-2-ylidenemethyl)}]phenylphosphate (882429-24-5) → C22H22Cl2F3NO5P(1-)*Na(1+) (882429-25-6)

Guidance literature:

With methanol; sodium methylate; at 20 ℃; for 0.5h;

upstream raw materials:

2-chloro-5-{1-(2,2,2-trifluoroethoxy-5'-chloro-tricyclo[3.3.1.1^3,7]dec-2-ylidenemethyl)}phenol

3-Hydroxypropionitrile

Downstream raw materials:

C₂₂H₂₂Cl₂F₃NO₅P^(1-)*Na⁽¹⁺⁾

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