Technology Process of C24H24FN7O4
There total 10 articles about C24H24FN7O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: N,N-dimethyl-formamide; trichlorophosphate / 1,2-dichloro-ethane / 3 h / 80 °C
2.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / 1,2-dimethoxyethane; water / 2 h / Inert atmosphere; Reflux
3.1: hydrogenchloride / 1,4-dioxane / 100 °C
4.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 5 °C / Inert atmosphere
4.2: 20 °C
5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C
With
hydrogenchloride; tetrakis(triphenylphosphine) palladium(0); tetrabutyl ammonium fluoride; sodium hydride; sodium carbonate; N,N-dimethyl-formamide; trichlorophosphate;
In
tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: hydrogen bromide; acetic acid / 3 h / 40 - 50 °C
2.1: N,N-dimethyl-formamide; trichlorophosphate / 1,2-dichloro-ethane / 3 h / 80 °C
3.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / 1,2-dimethoxyethane; water / 2 h / Inert atmosphere; Reflux
4.1: hydrogenchloride / 1,4-dioxane / 100 °C
5.1: sodium hydride / N,N-dimethyl-formamide / 0.25 h / 5 °C / Inert atmosphere
5.2: 20 °C
6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C
With
hydrogenchloride; tetrakis(triphenylphosphine) palladium(0); tetrabutyl ammonium fluoride; hydrogen bromide; sodium hydride; sodium carbonate; acetic acid; N,N-dimethyl-formamide; trichlorophosphate;
In
tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;