8-(p-iodophenyl)octyl 2,3,4-tri-O-acetyl-6-O-allyloxycarbonyl-β-D-glucopyranoside

Base Information

Chemical Name:8-(p-iodophenyl)octyl 2,3,4-tri-O-acetyl-6-O-allyloxycarbonyl-β-D-glucopyranoside
CAS No.:1357000-55-5
Molecular Formula:C₃₀H₄₁IO₁₁
Molecular Weight:704.553
Hs Code.:

Synonyms:8-(p-iodophenyl)octyl 2,3,4-tri-O-acetyl-6-O-allyloxycarbonyl-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-(p-iodophenyl)octyl 2,3,4-tri-O-acetyl-6-O-allyloxycarbonyl-β-D-glucopyranoside

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Technology Process of 8-(p-iodophenyl)octyl 2,3,4-tri-O-acetyl-6-O-allyloxycarbonyl-β-D-glucopyranoside

There total 2 articles about 8-(p-iodophenyl)octyl 2,3,4-tri-O-acetyl-6-O-allyloxycarbonyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1357000-43-1
8-(p-iodophenyl) octanol

: C₁₈H₂₂Cl₃NO₁₁

: 1357000-55-5
8-(p-iodophenyl)octyl 2,3,4-tri-O-acetyl-6-O-allyloxycarbonyl-β-D-glucopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -20 ℃; for 4h;
DOI:10.3987/COM-11-12332

Reference yield:

: 10472-97-6
8-phenyloctan-1-ol

: 1357000-55-5
8-(p-iodophenyl)octyl 2,3,4-tri-O-acetyl-6-O-allyloxycarbonyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: N-iodo-succinimide; trifluorormethanesulfonic acid / dichloromethane / 8 h / 20 °C

2: boron trifluoride diethyl etherate / dichloromethane / 4 h / -20 °C

With N-iodo-succinimide; trifluorormethanesulfonic acid; boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.3987/COM-11-12332

Reference yield: 94.0%

: 1357000-55-5
8-(p-iodophenyl)octyl 2,3,4-tri-O-acetyl-6-O-allyloxycarbonyl-β-D-glucopyranoside

: 1357000-57-7
8-(p-iodophenyl)octyl 2,3,4-tri-O-acetyl-β-D-glucopyranoside

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; formic acid; triphenylphosphine; In tetrahydrofuran; for 1h;
DOI:10.3987/COM-11-12332