phenyl 3,4,6-tri-O-acetyl-2-O--α-D-gluco-1-thiopyranoside

Base Information

Chemical Name:phenyl 3,4,6-tri-O-acetyl-2-O--α-D-gluco-1-thiopyranoside
CAS No.:143206-86-4
Molecular Formula:C₂₄H₃₆O₉SSi
Molecular Weight:528.696
Hs Code.:

phenyl 3,4,6-tri-O-acetyl-2-O-<tert-butoxy(dimethyl)silyl>-α-D-gluco-1-thiopyranoside

Synonyms:phenyl 3,4,6-tri-O-acetyl-2-O--α-D-gluco-1-thiopyranoside

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Chemical Property of phenyl 3,4,6-tri-O-acetyl-2-O--α-D-gluco-1-thiopyranoside

Chemical Property:

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Technology Process of phenyl 3,4,6-tri-O-acetyl-2-O--α-D-gluco-1-thiopyranoside

There total 4 articles about phenyl 3,4,6-tri-O-acetyl-2-O--α-D-gluco-1-thiopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 58566-07-7
tert-butoxy(dimethyl)silyl chloride

: 143206-82-0
phenyl 3,4,6-tri-O-acetyl-α-D-gluco-1-thiopyranoside

: 143206-86-4
phenyl 3,4,6-tri-O-acetyl-2-O--α-D-gluco-1-thiopyranoside

Guidance literature:: With pyridine; In tetrahydrofuran; for 2h;

Reference yield:

: 4451-37-0
3,4,6-tri-O-acetyl-β-D-glucopyranosyl chloride

: 143206-86-4
phenyl 3,4,6-tri-O-acetyl-2-O--α-D-gluco-1-thiopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) potassium / 1.) MeOH, -78 deg C₅ min, 2.) MeOH, 25 deg C, 4 h

2: 76 percent / pyridine / tetrahydrofuran / 2 h

With pyridine; potassium; In tetrahydrofuran;

Reference yield:

: 108-98-5
thiophenol

: 143206-86-4
phenyl 3,4,6-tri-O-acetyl-2-O--α-D-gluco-1-thiopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) potassium / 1.) MeOH, -78 deg C₅ min, 2.) MeOH, 25 deg C, 4 h

2: 76 percent / pyridine / tetrahydrofuran / 2 h

With pyridine; potassium; In tetrahydrofuran;