3,7,11-tris[N-(3,4-dimethoxybenzoyl)-(3-aminopropyl)]-3,7,11,17-tetraazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene

Base Information

• Chemical Name: 3,7,11-tris[N-(3,4-dimethoxybenzoyl)-(3-aminopropyl)]-3,7,11,17-tetraazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene
• CAS No.: 1010817-73-8
• Molecular Formula: C₄₉H₆₇N₇O₉
• Molecular Weight: 898.112

Synonyms:3,7,11-tris[N-(3,4-dimethoxybenzoyl)-(3-aminopropyl)]-3,7,11,17-tetraazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene

Chemical Property of 3,7,11-tris[N-(3,4-dimethoxybenzoyl)-(3-aminopropyl)]-3,7,11,17-tetraazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene

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Technology Process of 3,7,11-tris[N-(3,4-dimethoxybenzoyl)-(3-aminopropyl)]-3,7,11,17-tetraazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene

There total 1 articles about 3,7,11-tris[N-(3,4-dimethoxybenzoyl)-(3-aminopropyl)]-3,7,11,17-tetraazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

3,7,11-tris(3-aminopropyl)-3,7,11,17-tetraazabicyclo[11.3.1]-heptadeca-1(17),13,15-triene (912540-90-0) + 3,4-dimethoxybenzoic acid chloride (3535-37-3) → 3,7,11-tris[N-(3,4-dimethoxybenzoyl)-(3-aminopropyl)]-3,7,11,17-tetraazabicyclo[11.3.1]heptadeca-1(17),13,15-triene (1010817-73-8)

Guidance literature:

With sodium hydroxide; In dichloromethane; water; for 2h;

DOI:10.1039/b712916e

Reference yield: 56.0%

3,7,11-tris[N-(3,4-dimethoxybenzoyl)-(3-aminopropyl)]-3,7,11,17-tetraazabicyclo[11.3.1]heptadeca-1(17),13,15-triene (1010817-73-8) → 3,7,11-tris[N-(3,4-dihydroxybenzoyl)-(3-aminopropyl)]-3,7,11,17-tetraazabicyclo[11.3.1]heptadeca-1(17),13,15-triene (1010817-72-7)

Guidance literature:

With boron tribromide; In dichloromethane; at 20 ℃; for 48h;

DOI:10.1039/b712916e

upstream raw materials:

3,7,11-tris(3-aminopropyl)-3,7,11,17-tetraazabicyclo[11.3.1]-heptadeca-1⁽¹⁷⁾,13,15-triene

3,4-dimethoxybenzoic acid chloride

Downstream raw materials:

3,7,11-tris[N-(3,4-dihydroxybenzoyl)-(3-aminopropyl)]-3,7,11,17-tetraazabicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene

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