butyric acid 5-benzenesulfonyl-2-(tert-butyl-diphenyl-silanyloxy)-pentyl ester

Base Information

Chemical Name:butyric acid 5-benzenesulfonyl-2-(tert-butyl-diphenyl-silanyloxy)-pentyl ester
CAS No.:363625-21-2
Molecular Formula:C₃₁H₄₀O₅SSi
Molecular Weight:552.807
Hs Code.:

butyric acid 5-benzenesulfonyl-2-(<i>tert</i>-butyl-diphenyl-silanyloxy)-pentyl ester

Synonyms:butyric acid 5-benzenesulfonyl-2-(tert-butyl-diphenyl-silanyloxy)-pentyl ester

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Chemical Property of butyric acid 5-benzenesulfonyl-2-(tert-butyl-diphenyl-silanyloxy)-pentyl ester

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Technology Process of butyric acid 5-benzenesulfonyl-2-(tert-butyl-diphenyl-silanyloxy)-pentyl ester

There total 3 articles about butyric acid 5-benzenesulfonyl-2-(tert-butyl-diphenyl-silanyloxy)-pentyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 363625-20-1
Butyric acid (R)-5-benzenesulfonyl-2-hydroxy-pentyl ester

: 363625-21-2
butyric acid 5-benzenesulfonyl-2-(tert-butyl-diphenyl-silanyloxy)-pentyl ester

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(01)00856-5

Reference yield:

: 67100-19-0
(3-benzenesulfonyl-propyl)-oxirane

: 363625-21-2
butyric acid 5-benzenesulfonyl-2-(tert-butyl-diphenyl-silanyloxy)-pentyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: (S,S)-salen(Co)III(OAc); H₂O / tetrahydrofuran / 20 °C

2: 91 percent / Et₃N; Bu₂SnO / CH₂Cl₂ / 0 °C

3: 92 percent / imidazole / dimethylformamide

With 1H-imidazole; (S,S)-salen(Co)III(OAc); water; di(n-butyl)tin oxide; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(01)00856-5

Reference yield:

: 363625-00-7
(R)-5-Benzenesulfonyl-pentane-1,2-diol

: 363625-21-2
butyric acid 5-benzenesulfonyl-2-(tert-butyl-diphenyl-silanyloxy)-pentyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / Et₃N; Bu₂SnO / CH₂Cl₂ / 0 °C

2: 92 percent / imidazole / dimethylformamide

With 1H-imidazole; di(n-butyl)tin oxide; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(01)00856-5