1-[2-hydroxy-4-methoxy-5-(4-nitrophenylazo)phenyl]-1-phenylmethanone

Base Information

• Chemical Name: 1-[2-hydroxy-4-methoxy-5-(4-nitrophenylazo)phenyl]-1-phenylmethanone
• CAS No.: 1243203-30-6
• Molecular Formula: C₂₀H₁₅N₃O₅
• Molecular Weight: 377.356
• Mol file: 1243203-30-6.mol

Synonyms:1-[2-hydroxy-4-methoxy-5-(4-nitrophenylazo)phenyl]-1-phenylmethanone

Chemical Property of 1-[2-hydroxy-4-methoxy-5-(4-nitrophenylazo)phenyl]-1-phenylmethanone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-[2-hydroxy-4-methoxy-5-(4-nitrophenylazo)phenyl]-1-phenylmethanone

There total 2 articles about 1-[2-hydroxy-4-methoxy-5-(4-nitrophenylazo)phenyl]-1-phenylmethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

Benzophenone-3 (131-57-7,897050-18-9) + 4-nitro-aniline (100-01-6,104810-17-5) → 1-[2-hydroxy-4-methoxy-5-(4-nitrophenylazo)phenyl]-1-phenylmethanone (1243203-30-6)

Guidance literature:

4-nitro-aniline; With hydrogenchloride; sodium nitrite; In water; at 0 - 5 ℃;

Benzophenone-3; In water; at 0 - 5 ℃; Alkaline conditions;

Reference yield:

2-hydroxy-4-methoxybenzophenone-5-sulfonic acid (4065-45-6) + 4-nitro-aniline (100-01-6,104810-17-5) → 1-[2-hydroxy-4-methoxy-5-(4-nitrophenylazo)phenyl]-1-phenylmethanone (1243203-30-6)

Guidance literature:

4-nitro-aniline; With hydrogenchloride; In water; at 70 ℃; for 0.5h;

With sodium nitrite; In water; at 0 - 5 ℃;

2-hydroxy-4-methoxybenzophenone-5-sulfonic acid; Temperature; Solvent; regioselective reaction; Further stages;

DOI:10.1016/j.cclet.2013.04.016

upstream raw materials:

Benzophenone-3

4-nitro-aniline

2-hydroxy-4-methoxybenzophenone-5-sulfonic acid