5-<2-(N-methyl-N-ethoxycarbonylamino)vinyl>-1,3-diphenyl-1,2,4-triazoleN

Base Information

Chemical Name:5-<2-(N-methyl-N-ethoxycarbonylamino)vinyl>-1,3-diphenyl-1,2,4-triazoleN
CAS No.:107835-25-6
Molecular Formula:C₂₀H₂₀N₄O₂
Molecular Weight:348.404
Hs Code.:

Synonyms:5-<2-(N-methyl-N-ethoxycarbonylamino)vinyl>-1,3-diphenyl-1,2,4-triazoleN

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Chemical Property of 5-<2-(N-methyl-N-ethoxycarbonylamino)vinyl>-1,3-diphenyl-1,2,4-triazoleN

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Technology Process of 5-<2-(N-methyl-N-ethoxycarbonylamino)vinyl>-1,3-diphenyl-1,2,4-triazoleN

There total 5 articles about 5-<2-(N-methyl-N-ethoxycarbonylamino)vinyl>-1,3-diphenyl-1,2,4-triazoleN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.4%

: 6-Methyl-1,3-diphenyl-5,6-dihydro-5-oxopyrimido<4,3-c>triazolium chloride

: 107835-25-6
5-<2-(N-methyl-N-ethoxycarbonylamino)vinyl>-1,3-diphenyl-1,2,4-triazoleN

Guidance literature:: With sodium hydroxide; In ethanol; at 20 ℃; for 0.166667h;
DOI:10.1007/BF00519534

Reference yield: 32.8%

: 107835-22-3
1-Methyl-3-(phenylbenzhydrazonoyl)uracil

: 3346-44-9,118946-49-9
2,5-diphenyl-2,4-dihydro-3H-1,2,4-triazol-3-one

: 107835-25-6
5-<2-(N-methyl-N-ethoxycarbonylamino)vinyl>-1,3-diphenyl-1,2,4-triazoleN

Guidance literature:: With triethylamine; In ethanol; for 60h; Heating;
DOI:10.1007/BF00519534

Reference yield:

: 615-77-0
1-methyluracil

: 107835-25-6
5-<2-(N-methyl-N-ethoxycarbonylamino)vinyl>-1,3-diphenyl-1,2,4-triazoleN

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / 1N aq. NaOH / ethanol / 1.5 h / 20 °C

2: 51.7 percent / Et₃N / ethanol / 60 h / Heating

With sodium hydroxide; triethylamine; In ethanol;
DOI:10.1007/BF00519534