cyclohexylmethyl-2-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranoside

Base Information

Chemical Name:cyclohexylmethyl-2-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranoside
CAS No.:118250-16-1
Molecular Formula:C₄₈H₆₁NO₁₄
Molecular Weight:876.011
Hs Code.:

Synonyms:cyclohexylmethyl-2-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranoside

Suppliers and Price of cyclohexylmethyl-2-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of cyclohexylmethyl-2-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of cyclohexylmethyl-2-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranoside

There total 4 articles about cyclohexylmethyl-2-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 70831-94-6
3,4,6-tri-O-acetyl-2-deoxy-2-phthalimido-D-glucopyranosyl bromide

: 118250-16-1
cyclohexylmethyl-2-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / silver trifluoromethanesulfonate, sym-collidine, molecular sieve (4 Angstroem) / CH₂Cl₂ / 1 h / Ambient temperature

2: 1) hydrazine hydrate; 2) pyridine / 1) methanol, reflux, 5 h; 2) 16 h

With pyridine; 2,4,6-trimethyl-pyridine; 4 A molecular sieve; silver trifluoromethanesulfonate; hydrazine hydrate; In dichloromethane;
DOI:10.1016/0008-6215(88)84115-6

Reference yield:

: 118250-05-8
(2S,3S,4R,5R,6R)-4,5-Bis-benzyloxy-6-benzyloxymethyl-2-cyclohexylmethoxy-tetrahydro-pyran-3-ol

: 118250-16-1
cyclohexylmethyl-2-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / silver trifluoromethanesulfonate, sym-collidine, molecular sieve (4 Angstroem) / CH₂Cl₂ / 1 h / Ambient temperature

2: 1) hydrazine hydrate; 2) pyridine / 1) methanol, reflux, 5 h; 2) 16 h

With pyridine; 2,4,6-trimethyl-pyridine; 4 A molecular sieve; silver trifluoromethanesulfonate; hydrazine hydrate; In dichloromethane;
DOI:10.1016/0008-6215(88)84115-6

Reference yield:

: 118249-99-3
cyclohexylmethyl 2-O-acetyl-3,4,6-tri-O-benzyl-β-D-mannopyranoside

: 118250-16-1
cyclohexylmethyl-2-O-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3,4,6-tri-O-benzyl-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / sodium methoxide / methanol

2: 74 percent / silver trifluoromethanesulfonate, sym-collidine, molecular sieve (4 Angstroem) / CH₂Cl₂ / 1 h / Ambient temperature

3: 1) hydrazine hydrate; 2) pyridine / 1) methanol, reflux, 5 h; 2) 16 h

With pyridine; 2,4,6-trimethyl-pyridine; 4 A molecular sieve; sodium methylate; silver trifluoromethanesulfonate; hydrazine hydrate; In methanol; dichloromethane;
DOI:10.1016/0008-6215(88)84115-6