Technology Process of C17H22O2S2
There total 7 articles about C17H22O2S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
boron trifluoride diethyl etherate;
In
dichloromethane;
at 0 - 20 ℃;
Inert atmosphere;
DOI:10.1021/ol5000988
- Guidance literature:
-
Multi-step reaction with 5 steps
1: bis(η3-allyl-μ-chloropalladium(II)); 1,1'-bis-(diphenylphosphino)ferrocene; pyrrolidine / methanol / 12 h / 20 °C / Inert atmosphere
2: potassium carbonate; sodium periodate; potassium permanganate / water; tert-butyl alcohol / 0 - 20 °C / Inert atmosphere
3: thionyl chloride / methanol / -10 - 20 °C / Inert atmosphere
4: 20 °C / Inert atmosphere
5: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C / Inert atmosphere
With
pyrrolidine; 1,1'-bis-(diphenylphosphino)ferrocene; potassium permanganate; sodium periodate; thionyl chloride; bis(η3-allyl-μ-chloropalladium(II)); boron trifluoride diethyl etherate; potassium carbonate;
In
methanol; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/ol5000988
- Guidance literature:
-
Multi-step reaction with 5 steps
1: bis(η3-allyl-μ-chloropalladium(II)); 1,1'-bis-(diphenylphosphino)ferrocene; pyrrolidine / methanol / 8 h / 20 °C / Inert atmosphere
2: potassium carbonate; sodium periodate; potassium permanganate / water; tert-butyl alcohol / 0 - 20 °C / Inert atmosphere
3: thionyl chloride / methanol / -10 - 20 °C / Inert atmosphere
4: 20 °C / Inert atmosphere
5: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C / Inert atmosphere
With
pyrrolidine; 1,1'-bis-(diphenylphosphino)ferrocene; potassium permanganate; sodium periodate; thionyl chloride; bis(η3-allyl-μ-chloropalladium(II)); boron trifluoride diethyl etherate; potassium carbonate;
In
methanol; dichloromethane; water; tert-butyl alcohol;
DOI:10.1021/ol5000988