2-(10-methyl-6,7,8,9-tetrahydropyrido[1,2-a]indol-6-yl)-1-phenylethanone

Base Information

Chemical Name:2-(10-methyl-6,7,8,9-tetrahydropyrido[1,2-a]indol-6-yl)-1-phenylethanone
CAS No.:1260083-00-8
Molecular Formula:C₂₁H₂₁NO
Molecular Weight:303.404
Hs Code.:

Synonyms:2-(10-methyl-6,7,8,9-tetrahydropyrido[1,2-a]indol-6-yl)-1-phenylethanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(10-methyl-6,7,8,9-tetrahydropyrido[1,2-a]indol-6-yl)-1-phenylethanone

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Technology Process of 2-(10-methyl-6,7,8,9-tetrahydropyrido[1,2-a]indol-6-yl)-1-phenylethanone

There total 2 articles about 2-(10-methyl-6,7,8,9-tetrahydropyrido[1,2-a]indol-6-yl)-1-phenylethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1260082-99-2
(E)-6-(3-methyl-1H-indol-2-yl)-1-phenylhex-2-en-1-one

: 1260083-00-8
2-(10-methyl-6,7,8,9-tetrahydropyrido[1,2-a]indol-6-yl)-1-phenylethanone

Guidance literature:: With (S)-3,3'-bis(triphenylsilyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate; In toluene; at -20 ℃; for 17h; optical yield given as %ee; enantioselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1002/anie.201003919

Reference yield: 89.0%

: 1260083-03-1
3-methyl-2-(pent-4-enyl)-1H-indole

: 768-03-6,26742-84-7
Phenyl vinyl ketone

: 1260083-00-8
2-(10-methyl-6,7,8,9-tetrahydropyrido[1,2-a]indol-6-yl)-1-phenylethanone

Guidance literature:: With 1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene[2-(iso-propoxy)-5-(N,N-dimethylaminosulfonyl)phenyl]methylene ruthenium(II) dichloride; (S)-3,3'-bis(triphenylsilyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate; In toluene; at 50 ℃; optical yield given as %ee; enantioselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1002/anie.201003919