C₃₆H₄₆N₂O₁₀SSi

Base Information

Chemical Name:C₃₆H₄₆N₂O₁₀SSi
CAS No.:1574543-71-7
Molecular Formula:C₃₆H₄₆N₂O₁₀SSi
Molecular Weight:726.92
Hs Code.:

C<sub>36</sub>H<sub>46</sub>N<sub>2</sub>O<sub>10</sub>SSi

Synonyms:C₃₆H₄₆N₂O₁₀SSi

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Chemical Property of C₃₆H₄₆N₂O₁₀SSi

Chemical Property:

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Technology Process of C₃₆H₄₆N₂O₁₀SSi

There total 12 articles about C₃₆H₄₆N₂O₁₀SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1574543-55-7
(3aR,4S,6S,6aS)-6a-(tert-butyldiphenylsilyloxy)methyl-4-(2,2-dimethoxyethyl)-6-(methoxymethoxy)hexahydrocyclopenta[c]pyrrol-1(2H)-one

: 1694-92-4
2-Nitrobenzenesulfonyl chloride

: 1574543-71-7
C₃₆H₄₆N₂O₁₀SSi

Guidance literature:: (3aR,4S,6S,6aS)-6a-(tert-butyldiphenylsilyloxy)methyl-4-(2,2-dimethoxyethyl)-6-(methoxymethoxy)hexahydrocyclopenta[c]pyrrol-1(2H)-one; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.0833333h; Inert atmosphere;

2-Nitrobenzenesulfonyl chloride; In tetrahydrofuran; at -78 - 0 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol5002973

Reference yield:

: 1574543-68-2
C₁₃H₁₆O₄

: 1574543-71-7
C₃₆H₄₆N₂O₁₀SSi

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium tris(acetoxy)borohydride / acetonitrile; acetic acid / 1 h / 0 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine; dmap / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

2.2: 12 h / 0 - 20 °C / Inert atmosphere

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; pyrrolidine / acetonitrile / 3 h / 50 °C

4.1: thionyl chloride / dichloromethane; N,N-dimethyl-formamide / 0.25 h / -30 - 20 °C / Inert atmosphere

4.2: 0.17 h / -20 - 10 °C

5.1: ozone / dichloromethane; methanol / 0.08 h / -78 °C

5.2: 4 h / -78 - 20 °C / Inert atmosphere

6.1: CSA / methanol / 24 h / 20 °C / Inert atmosphere

7.1: sodium cyanoborohydride / tetrahydrofuran; formic acid / 4 h / 0 - 20 °C / Inert atmosphere

8.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.08 h / -78 °C / Inert atmosphere

8.2: 2 h / -78 - 0 °C / Inert atmosphere

With pyrrolidine; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; sodium tris(acetoxy)borohydride; sodium cyanoborohydride; ozone; N-ethyl-N,N-diisopropylamine; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; formic acid; dichloromethane; acetic acid; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ol5002973

Reference yield:

: 1574543-51-3
(1S,2S,3aR,6aS)-1-(tert-butyldiphenylsilyloxy)methyl-2-methoxymethoxy-1,2,3,3a,4,6a-hexahydropentalene-1-carboxylic acid

: 1574543-71-7
C₃₆H₄₆N₂O₁₀SSi

Guidance literature:: Multi-step reaction with 5 steps

1.1: thionyl chloride / dichloromethane; N,N-dimethyl-formamide / 0.25 h / -30 - 20 °C / Inert atmosphere

1.2: 0.17 h / -20 - 10 °C

2.1: ozone / dichloromethane; methanol / 0.08 h / -78 °C

2.2: 4 h / -78 - 20 °C / Inert atmosphere

3.1: CSA / methanol / 24 h / 20 °C / Inert atmosphere

4.1: sodium cyanoborohydride / tetrahydrofuran; formic acid / 4 h / 0 - 20 °C / Inert atmosphere

5.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.08 h / -78 °C / Inert atmosphere

5.2: 2 h / -78 - 0 °C / Inert atmosphere

With thionyl chloride; sodium cyanoborohydride; ozone; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; formic acid; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol5002973