{(C₄H₉)4N}{NiI₃Triphenylphosphin}

Base Information

Chemical Name:{(C₄H₉)4N}{NiI₃Triphenylphosphin}
CAS No.:14320-07-1
Molecular Formula:C₁₆H₃₆N*C₁₈H₁₅I₃NiP
Molecular Weight:944.163
Hs Code.:

{(C<sub>4</sub>H<sub>9</sub>)4N}{NiI<sub>3</sub>Triphenylphosphin}

Synonyms:{(C₄H₉)4N}{NiI₃Triphenylphosphin}

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Chemical Property of {(C₄H₉)4N}{NiI₃Triphenylphosphin}

Chemical Property:

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Technology Process of {(C₄H₉)4N}{NiI₃Triphenylphosphin}

There total 11 articles about {(C₄H₉)4N}{NiI₃Triphenylphosphin} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: nickel(II) iodide hexahydrate

: 311-28-4
tetra-(n-butyl)ammonium iodide

: 603-35-0
triphenylphosphine

: 14320-07-1
{(C₄H₉)4N}{NiI₃Triphenylphosphin}

Guidance literature:: In diethyl ether; butan-1-ol; dehydration of NiI2*6H2O with dimethoxy propane, stirring for 10 h at 40°C; washing with abs. ether, drying in vac. over P2O5;
DOI:10.1021/ja00965a016

Reference yield: 19.0%

: 13462-90-3
nickel(II) iodide

: 311-28-4
tetra-(n-butyl)ammonium iodide

: 603-35-0
triphenylphosphine

: 14320-07-1
{(C₄H₉)4N}{NiI₃Triphenylphosphin}

Guidance literature:: In butan-1-ol; evapn. at low pressure; washing with butanol, drying in vac.;
DOI:10.1021/ja01463a021 DOI:10.1021/ja01496a074

Reference yield:

: {C₁₈H₁₅PC₆H₅}{NiBr₂Cl(Triphenylphosphin)}

: 14320-07-1
{(C₄H₉)4N}{NiI₃Triphenylphosphin}

Guidance literature:: Multi-step reaction with 2 steps

1: methanol

2: butan-1-ol; diethyl ether

With methanol; In diethyl ether; butan-1-ol;