1-(2-(benzo[1,3]dioxol-5-yl)ethyl)-3-(toluene-4-sulfonyl)piperidine-2,6-dione

Base Information

Chemical Name:1-(2-(benzo[1,3]dioxol-5-yl)ethyl)-3-(toluene-4-sulfonyl)piperidine-2,6-dione
CAS No.:1021494-14-3
Molecular Formula:C₂₁H₂₁NO₆S
Molecular Weight:415.467
Hs Code.:

Synonyms:1-(2-(benzo[1,3]dioxol-5-yl)ethyl)-3-(toluene-4-sulfonyl)piperidine-2,6-dione

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Chemical Property of 1-(2-(benzo[1,3]dioxol-5-yl)ethyl)-3-(toluene-4-sulfonyl)piperidine-2,6-dione

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Technology Process of 1-(2-(benzo[1,3]dioxol-5-yl)ethyl)-3-(toluene-4-sulfonyl)piperidine-2,6-dione

There total 1 articles about 1-(2-(benzo[1,3]dioxol-5-yl)ethyl)-3-(toluene-4-sulfonyl)piperidine-2,6-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1021494-15-4
C₁₈H₁₉NO₅S

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 1021494-14-3
1-(2-(benzo[1,3]dioxol-5-yl)ethyl)-3-(toluene-4-sulfonyl)piperidine-2,6-dione

Guidance literature:: C₁₈H₁₉NO₅S; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.5h;

acrylic acid methyl ester; In tetrahydrofuran; at 20 ℃; for 8h; Further stages.;
DOI:10.1016/j.tet.2008.01.119

Reference yield:

: 1021494-14-3
1-(2-(benzo[1,3]dioxol-5-yl)ethyl)-3-(toluene-4-sulfonyl)piperidine-2,6-dione

: C₂₁H₂₃NO₆S

Guidance literature:: 1-(2-(benzo[1,3]dioxol-5-yl)ethyl)-3-(toluene-4-sulfonyl)piperidine-2,6-dione; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 0.25h;

With lithium aluminium tetrahydride; In tetrahydrofuran; for 2h; Further stages.; cooling;
DOI:10.1016/j.tet.2008.01.119