C₆₆H₇₇N₉O₉S

Base Information

Chemical Name:C₆₆H₇₇N₉O₉S
CAS No.:1591626-71-9
Molecular Formula:C₆₆H₇₇N₉O₉S
Molecular Weight:1172.46
Hs Code.:

C<sub>66</sub>H<sub>77</sub>N<sub>9</sub>O<sub>9</sub>S

Synonyms:C₆₆H₇₇N₉O₉S

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Chemical Property of C₆₆H₇₇N₉O₉S

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Technology Process of C₆₆H₇₇N₉O₉S

There total 4 articles about C₆₆H₇₇N₉O₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1591626-70-8
C₃₂H₄₄N₄O₆

: 1421686-62-5
C₃₄H₃₅N₅O₄S

: 1591626-71-9
C₆₆H₇₇N₉O₉S

Guidance literature:: With N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃; for 48h;
DOI:10.1021/ja5022415

Reference yield:

: 2577-40-4
Phe-Phe

: 1591626-71-9
C₆₆H₇₇N₉O₉S

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid / water / 24 h / Reflux

2: bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 24 h / 20 °C

3: water; sodium hydroxide / methanol / 2 h / 20 °C

4: bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 48 h / 20 °C

With sulfuric acid; water; N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; sodium hydroxide; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/ja5022415

Reference yield:

: 67247-04-5
Phe-Phe-OEt

: 1591626-71-9
C₆₆H₇₇N₉O₉S

Guidance literature:: Multi-step reaction with 3 steps

1: bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 24 h / 20 °C

2: water; sodium hydroxide / methanol / 2 h / 20 °C

3: bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 48 h / 20 °C

With water; N-ethyl-N,N-diisopropylamine; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate; sodium hydroxide; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/ja5022415