Z-L-phenylalanine DCHA salt

Base Information

Chemical Name:Z-L-phenylalanine DCHA salt
CAS No.:87072-42-2
Molecular Formula:C₁₂H₂₃N*C₁₇H₁₇NO₄
Molecular Weight:480.648
Hs Code.:

Synonyms:Z-L-phenylalanine DCHA salt

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Chemical Property of Z-L-phenylalanine DCHA salt

Chemical Property:

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Technology Process of Z-L-phenylalanine DCHA salt

There total 2 articles about Z-L-phenylalanine DCHA salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 13139-17-8
N-(Benzyloxycarbonyloxy)succinimide

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 101-83-7
N-cyclohexyl-cyclohexanamine

: 87072-42-2
Z-L-phenylalanine DCHA salt

Guidance literature:: N-(Benzyloxycarbonyloxy)succinimide; L-phenylalanine; With sodium hydrogencarbonate; sodium carbonate; In water; acetone; at 20 ℃; for 3h;

N-cyclohexyl-cyclohexanamine; In water; isopropyl alcohol; acetone; at 20 ℃; for 9h;

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 501-53-1,94274-21-2
benzyl chloroformate

: 101-83-7
N-cyclohexyl-cyclohexanamine

: 87072-42-2
Z-L-phenylalanine DCHA salt

Guidance literature:: With sodium hydroxide; Multistep reaction; 1.) ca 5 deg C, 15 min 2.) ethyl acetate, Et₂O, 5 min;
DOI:10.1016/S0040-4020(01)87839-X

Reference yield:

: 87072-42-2
Z-L-phenylalanine DCHA salt

: H-Phe-Pro-Pro-Phe-Ile-Val-OH

Guidance literature:: Multi-step reaction with 3 steps

1: N-methylmorpholine / tetrahydrofuran / 0.25 h / -5 °C

2: N-methylmorpholine / dimethylformamide; tetrahydrofuran / 1) -5 deg C, 1 h, 2) RT, overnight

3: 97 percent / H₂ / palladium black

With 4-methyl-morpholine; hydrogen; palladium; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1246/bcsj.57.301