N-(2-amino-1-tert-butyl-3,3-dimethyl-butyl)-4-methyl-benzenesulfonamide

Base Information

Chemical Name:N-(2-amino-1-tert-butyl-3,3-dimethyl-butyl)-4-methyl-benzenesulfonamide
CAS No.:799261-86-2
Molecular Formula:C₁₇H₃₀N₂O₂S
Molecular Weight:326.503
Hs Code.:

<i>N</i>-(2-amino-1-<i>tert</i>-butyl-3,3-dimethyl-butyl)-4-methyl-benzenesulfonamide

Synonyms:N-(2-amino-1-tert-butyl-3,3-dimethyl-butyl)-4-methyl-benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-amino-1-tert-butyl-3,3-dimethyl-butyl)-4-methyl-benzenesulfonamide

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Technology Process of N-(2-amino-1-tert-butyl-3,3-dimethyl-butyl)-4-methyl-benzenesulfonamide

There total 4 articles about N-(2-amino-1-tert-butyl-3,3-dimethyl-butyl)-4-methyl-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 799261-65-7
(4S,5S)-trans-1-p-tolylsulfonyl-4,5-di-tert-butyl-2-imidazolidinone

: 799261-86-2
N-(2-amino-1-tert-butyl-3,3-dimethyl-butyl)-4-methyl-benzenesulfonamide

Guidance literature:: With barium dihydroxide; In ethanol; water; at 140 ℃; for 72h;
DOI:10.1016/j.tetlet.2004.08.164

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 799261-86-2
N-(2-amino-1-tert-butyl-3,3-dimethyl-butyl)-4-methyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: 79 percent / NaH / tetrahydrofuran / 4 h / 20 °C

2: 100 percent / LiBH₄; MeOH / tetrahydrofuran / 3 h / 20 °C

3: 69 percent / LiCl; BF₃*OEt₂ / tetrahydrofuran / 24 h / -30 °C

4: 73 percent / Ba(OH)2*8H₂O / ethanol; H₂O / 72 h / 140 °C

With methanol; barium dihydroxide; lithium borohydride; boron trifluoride diethyl etherate; sodium hydride; lithium chloride; In tetrahydrofuran; ethanol; water;
DOI:10.1016/j.tetlet.2004.08.164

Reference yield:

: 799261-63-5
(4S,5S)-5-tert-Butyl-4-methoxy-1-(toluene-4-sulfonyl)-imidazolidin-2-one

: 799261-86-2
N-(2-amino-1-tert-butyl-3,3-dimethyl-butyl)-4-methyl-benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / LiCl; BF₃*OEt₂ / tetrahydrofuran / 24 h / -30 °C

2: 73 percent / Ba(OH)2*8H₂O / ethanol; H₂O / 72 h / 140 °C

With barium dihydroxide; boron trifluoride diethyl etherate; lithium chloride; In tetrahydrofuran; ethanol; water;
DOI:10.1016/j.tetlet.2004.08.164